This study refers to the development and characterization of silver oxide nanoparticles obtained by X-ray diffraction, nanostructured silver oxide was used in order to calculate the micro strain and crystal size by Halder-Wagner method and by relying on X-ray diffraction diagram of the nonstructural silver oxide, where the results of the crystal size and the micro-strain were 4nm and 0.33 respectively. Other analysis techniques, such as the Size-strain plot, The X-ray diffraction study confirmed that the crystalline nature of silver oxide nanoparticles has a cubic structure. Through the X-ray diffraction results, the crystal size was calculated using Debye-Scherrer and Williamson-Hall methods. Halder-Wagner (HW), Size-strain plot, Debye –Scherrer’s and the Williamson-Hall methods were used to investigate the crystal size from the XRD peak broadening analysis. Moreover, the silver oxide particle size was calculated by the different methods where the values of crystal size. It was found that values of crystal size are 7.4166nm, 1.562525315, 2.285233333nm calculated by Williamson-Hall (W-H), Size-Strain Plot (SSP) and Halder method, respectively. The Sample was considered to determine physical and microstructural parameters such as strain, strain, and energy density.
X-ray diffractometers deliver the best quality diffraction data while being easy to use and adaptable to various applications. When X-ray photons strike electrons in materials, the incident photons scatter in a direction different from the incident beam; if the scattered beams do not change in wavelength, this is known as elastic scattering, which causes amplitude and intensity diffraction, leading to constructive interference. When the incident beam gives some of its energy to the electrons, the scattered beam's wavelength differs from the incident beam's wavelength, causing inelastic scattering, which leads to destructive interference and zero-intensity diffraction. In this study, The modified size-strain plot method was used to examine the pattern of x-ray diffraction lines (101),(121),(202),(042), and (242) for calcium titanate(CaTiO3) nanoparticles in this study. To calculate the new variables, the size strain plot method was created., X-ray line analysis and calculation of crystal size and lattice tension of calcium titanate oxide nanoparticles. It is used to calculate the crystal volume (44.7 nm) and to calculate the determination of network parameters such as the texture modulus (Tc), macro stress (MS), specific surface area (SSA), and dislocation density(η), respectively.
The Fourier method was developed to calculate other important variables in the crystalline structure, such a strain, which is equal to 7.4828 x 10−3 instead of the mean square strain and the energy density of the strain, which is equal to 2799614.7 dyne / cm2 and the stress equal to 7.4828 x 108 dyne/cm2. The results obtained from the Fourier method for calculating other parameters of the manganese oxide lattice for each peak of x-ray diffraction peaks such as the texture coefficient, its mean value equal to 0.99999 and the micro strains, which its mean value equal to 4.47 × 10−3 dislocation density, its mean value are equal to 37.3 (lines .m−2) and the specific surface area its mean value is equal to 19,58432 of crystalline volume. A comparison was also made between the values of the square of strain and the apparent strain.
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