The use of piezoelectric nanocomposite in detection and actuation applications for the development of electromechanical microsystems (MEMS) has become quite common over the last decade. In this paper, we present a flexible piezoelectric nanocomposite films, composed of lead zirconate titanate (PZT) nanoparticles, embedded in poly(vinylidene-difluoride hexafluoro propylene) (PVdF-HFP) matrix. Piezoelectric and ferroelectric properties evolution is proportional to the evolution of the crystalline β-phase. The evaluation of the interactions between PZT and PVdF- HFP, performed by Fourier transform infrared spectroscopy (FTIR), revealed a dramatic improvement in these characteristics over pure PVdF-HFP, and attributed to a better crystallinity of the PVdF-HFP matrix and uniform distribution of nanoparticles. These films nanocomposites were done by solvent casting method, with various concentrations of PZT. Results of these experiments indicate that the investigated thin films nanocomposites are appropriate for various applications in energy storage and energy harvesting application.
Natural indigo is hardly used anymore, replaced by synthetic indigo. Considered to be more powerful and more intense. The aim of this study is to optimize the method of extracting indigo carmine from the Isatis plant located in the Timhdit region of Morocco, during the fermentation period of the extracted liquid (pH = 10) and by adding 10% sugar it was possible to increase the yield by 0.5% indigo carmine blue powder to 0.9%. The main effect of applying centrifugation at 7000 rpm instead of conventional filtration is the reduction of the time from 30 min to 5 min as well as the reduction of the loss of traces of indigo in the filter papers by easily recovering the blue powder in the form of sediment in the centrifuge tubes. The extracted pigment is characterized by the infrared which confirmed the structure of the indigo carmine obtained, by visible UV spectroscopy, the maximum absorption of which is approximately 598 nm. This blue pigment was applied to the wool fibres by optimizing the dyeing procedure (T = 50 ° C and pH=10) with a 1/100 bath ratio and a 35 min soaking time. Dyed wool sample has reached a rigid fixation confirmed by the test for fastness washing 105-C06 and to friction 105 -X12.
The flexible piezoelectric nanocomposite films have attracted considerable interest for use in autonomous nanosystems, sensors and portable electronics. The effect of graphene oxide (GO) nanoparticles on the crystal structure, unique crystallization, mechanical behavior and significant improvement in piezoelectricity of polylactic acid (PLA) has been reported. Polylactic acid / graphene oxide (PLA/GO) nanocomposite films were prepared by the solvent casting technique using different percentages of GO. The different samples were characterized by Polarized optical microscope (POM), Fourier transformed infrared (FTIR) and X-ray diffraction analysis. The presence of β phase in nanocomposites and the enhancement of their piezoelectric properties were confirmed by FTIR and XRD analysis. These electroactive and biodegradable polymer nanocomposite thin films may be a potential candidate for the piezoelectric nanogenerators, energy storage devices and energy harvesting applications.
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