Through understanding that the fluid in the vortex fluidic device (VFD) housing an inclined rapidly rotating tube exhibits resonance behaviours from the confining boundaries of the glass surface and the...
Lateral slicing of micron length carbon nanotubes (CNTs) is effective on laser irradiation of the materials suspended within dynamic liquid thin films in a microfluidic vortex fluidic device (VFD). The method produces sliced CNTs with minimal defects in the absence of any chemical stabilizers, having broad length distributions centred at ca 190, 160 nm and 171 nm for single, double and multi walled CNTs respectively, as established using atomic force microscopy and supported by small angle neutron scattering solution data. Molecular dynamics simulations on a bent single walled carbon nanotube (SWCNT) with a radius of curvature of order 10 nm results in tearing across the tube upon heating, highlighting the role of shear forces which bend the tube forming strained bonds which are ruptured by the laser irradiation. CNT slicing occurs with the VFD operating in both the confined mode for a finite volume of liquid and continuous flow for scalability purposes.
Mixing immiscible liquids typically requires the use of auxiliary substances including phase transfer catalysts, microgels, surfactants, complex polymers and nano- particles and/or micromixers. Centrifugally separated immiscible liquids of different densities...
Thin film microfluidic shearing of a mixture of toluene dispersed single walled carbon nanotubes (SWCNTs) and water in a vortex fluidic device results in SWCNT nanorings (and related structures), diameters 100 to 200 nm or 300 to 700 nm, for respectively 10 mm or 20 mm diameter rotating tubes.
A method for controlling the self-assembly of fullerene C molecules into nanotubules in the fcc phase, devoid of entrapped solvent, has been established in a thin film microfluidic device. The micron length C nanotubules, with individual hollow diameters of 100 to 400 nm, are formed under continuous flow processing during high shear micromixing of water and a toluene solution of the fullerene, in the absence of surfactant, and without the need for further down-stream processing. TEM revealed pores on the surface of the nanotubes, and the isolated material has a much higher response to small molecule sensing than that for analogous material formed using multistep batch processing.
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