The present study concentrated on porous geopolymer composites (between calcined clay and metakaolin) using hydrogen peroxide as a pore generation agent. To reduce as well as recycle the waste from a factory, calcined clay waste was used as starting material. The geopolymer was synthesized via a geopolymerization method by a reaction with an alkaline solution, using the ceramic waste and metakaolin as raw materials. Different amount of olive oil (0–15 wt%) were added to the samples. The olive oil affected the pore formation of the geopolymers. The effects of olive oil, a surfactant, on the properties of the geopolymer composites were investigated. Apparent density and compressive strength of the samples tended to decrease with the additive, while water absorption and total porosity had the opposite effect. However, a variation in the apparent density and water absorption values was observed, due to the formation of closed pores in the samples. The trend of compressive strength value was related with total porosity. A model for pore formation was proposed in this work. The results suggest that this material can be used as a geopolymer foam.
The effect of argon (Ar) and oxygen (O2) gases as well as the treatment times on the properties of modified bamboo fibers using dielectric barrier discharge (DBD) plasma at generated power of 180 W were investigated. The plasma treatment of bamboo fibers with inert gases leads to the generation of ions and radicals on the fiber surface. Fourier transform-infrared spectroscopy (FTIR) confirmed that the functional groups of lignin and hemicellulose were reduced owing to the removal of the amorphous portion of the fibers by plasma etching. X-ray diffraction analysis (XRD) results in an increased crystallinity percentage. X-ray photoelectron spectroscopy (XPS) results showed the oxygen/carbon (O/C) atomic concentration ratio increased with increasing treatment time. The fiber weight loss percentage increased with increased treatment time. Scanning electron microscopy (SEM) images showed that partial etching of the fiber surface led to a higher surface roughness and area and that the Ar + O2 gas plasma treatment provided more surface etching than the Ar gas treatment because of the oxidation reaction of the O2 plasma. The mechanical properties of fiber-reinforced epoxy (FRE) matrix composites revealed that the F(tr)RE-Ar (30) samples showed a high tensile strength, whereas the mechanical properties of the F(tr)RE-Ar + O2 sample decreased with increased treatment time.
Porous alumino-siliceous (PAS) materials are attractive for use in a wide variety of construction and adsorption materials. In the present study, the porous alumino-siliceous materials were synthesized by a geopolymerization method in a reaction from ceramic waste, metakaolin, and an alkaline solution, H 2 O 2 (as a foaming agent) and either pork lard or butter (surfactants). Different amounts of the surfactants (2.5-15 wt%) were added to the samples. The pore shape in the PAS materials was affected by the type of surfactant used. PAS materials with small open pores and high porosity were successfully fabricated with butter as a surfactant. The compressive strength value trend was related to total porosity. The relationship between compressive strength and porosity was found to be consistent with a model proposed by Ryshkewitch. The results suggest that this material can be used as a foam material.
The present study focuses on the new application of geopolymer ceramic composites as substrate cultures, resulting from the geopolymer properties being similar to those of the substrate cultures such as water absorption, non-biodegradation, high porosity, and light weight. The geopolymers were synthesized from ceramic wastes and metakaolin using the geopolymerization method via a reaction with an alkaline solution. To compare usefulness for substrate culture applications, the porosity of different samples was varied. Moreover, the properties of all samples were investigated using an additional method of verification. The chemical characteristics were evaluated by FT-IR spectroscopy. The microstructures, pore sizes, pore distributions and surface areas of the pores were examined with image analysis using scanning electron microscopy (SEM). The densities were determined using the Archimedes’ method. The porosity and water absorption were also measured. The mechanical properties were investigated by using a compression testing machine.
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