Abstract. High temperature gas nitriding performed on AISI 316L at the temperature of 1200°C. The microstructure of treated AISI 316L samples were observed to identify the formation of the microstructure of nitrided surface layer. The grain size of austenite tends to be enlarged when the nitriding time increases, but the austenite single phase structure is maintained even after the long-time solution nitriding. Using microhardness testing, the hardness values drop to the center of the samples. The increase in surface hardness is due to the high nitrogen concentration at or near the surface. At 245HV, the graph of the effective duration of nitriding process was plotted to achieve the maximum depth of nitrogen diffuse under the surface. Using Sigma Plot software best fit lines of the experimental result found and plotted to find out effective duration of nitriding equation as Y=1.9491(1-0.7947 x ), where Y is the thickness of nitrided layer below the surface and X is duration of nitriding process. Based on this equation, the duration of gas nitriding process can be estimated to produce desired thickness of nitrided layer.
Lack of information about the formulation and fabrication process of starch polymer foam and lack of study in the shock absorption ability of starch polymer foam were the reasons this research was executed. In this project starch polymer foam was produced to be used as cushioning material for packaging. Starch polymer foam were developed from starch, polyvinyl alcohol (PVA), urea, citric acid, and deionised water. Water amount with drying and curing process were the variables manipulated to produce the best starch polymer foam. It was determined then, that the optimized ratio of starch:PVA:citric acid was 1:1:4. The amount of water used was 10 ml/gram of starch/PVA weight. The suitable foaming mixing was done at a speed of 1500 rpm for 40 minutes. Drying process was done at 70°C for 24 hours, followed by curing process at 100°C for 1 hour to produce closed-cell foam. While for the open-cell foam, the foam was dried and cured at 100ºC for 6 hours. The open-cell and closed-cell foams produced were cut to 6 cm height x 6 cm width x 0.5 cm thick. The average density was calculated and then the foams were subjected to weight drop destructive test. The test was done by placing a foam on top of a piece of mirror, and a weight is dropped onto the foam, with increasing height until the mirror break. Three weights were used with mass of 50 g, 100 g and 200 g. The starch foams were compared to polyurethane and polystyrene foams in terms of the minimum height that can cause the mirror to break. The results showed that starch closed-cell foam absorbed the highest impact energy followed by polystyrene foam, starch open-cell foam and polyurethane foam.
Abstract. This paper present mathematical model which developed to predict the nitrided layer thickness (case depth) of gas nitrided and plasma nitrided austenitic stainless steel according to Fick's first law for pure iron by adapting and manipulating the Hosseini's model to fit the diffusion mechanism where nitrided structure formed by nitrided AISI 316L austenitic stainless steel. The mathematical model later tested against various actual gas nitriding and plasma nitriding experimental results with varying nitriding temperature and nitriding duration to see whether the model managed to successfully predict the nitrided layer thickness. This model predicted the coexistence of ε-Fe2-3N and γ΄-Fe4N under the present nitriding process parameters. After the validation process, it is proven that the mathematical model managed to predict the nitrided layer growth of the gas nitrided and plasma nitrided of AISI 316L SS up to high degree of accuracy.
Abstract. Martensitic stainless steels are commonly used for fabricating components. For many applications, an increase in surface hardness and wear resistance can be beneficial to improve performance and extend service life. However, the improvement in hardness of martensitic steels is usually accompanied by a reduction in corrosion strength. The objective of this study is to investigate the effects of nitriding on AISI 420 martensitic stainless steel, in terms of microstructure and corrosion propagation behavior. The results indicate that the microstructure and phase composition as well as corrosion resistance were influenced by nitriding temperatures.
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