The characteristic volatiles of light, medium and dark roasted Turkish-style boiled coffee brews were studied by head space solid-phase micro extraction/gas chromatography-mass spectrometry and sensory flavour profile analysis. Sixty five volatile compounds, including furans, pyrazines, pyrroles, phenols, pyridines, ketones, oximes, alcohols, aldehydes, thiophenes, benzenes and terpenes, were isolated from Turkish-style boiled coffee samples. The flavour profile analysis showed Turkish coffee brews as roasted/burnt, spicy, bitter, acidic, sweet, salty, astringent (dry), woody, fermented, earthy and tobacco-like flavour characteristics. It was concluded that Turkish coffee was rich in furans, pyrazines, pyrroles and phenols giving its roasted/burnt, spicy, woody and fermented flavour characteristics.