Soils comprise the largest pool of terrestrial carbon yet have lost significant stocks due to human activity. Changes to land management in cropland and grazing systems present opportunities to sequester carbon in soils at large scales. Uncertainty in the magnitude of this potential impact is largely driven by the difficulties and costs associated with measuring near-surface (0–30 cm) soil carbon concentrations; a key component of soil carbon stock assessments. Many techniques exist to optimize sampling, yet few studies have compared these techniques at varying sample intensities. In this study, we performed ex-ante, high-intensity sampling for soil carbon concentrations at four farms in the eastern United States. We used post hoc Monte-Carlo bootstrapping to investigate the most efficient sampling approaches for soil carbon inventory: K-means stratification, Conditioned Latin Hypercube Sampling (cLHS), simple random, and regular grid. No two study sites displayed similar patterns across all sampling techniques, although cLHS and grid emerged as the most efficient sampling schemes across all sites and strata sizes. The number of strata chosen when using K-means stratification can have a significant impact on sample efficiency, and we caution future inventories from using small strata n, while avoiding even allocation of sample between strata. Our findings reinforce the need for adaptive sampling methodologies where initial site inventory can inform primary, robust inventory with site-specific sampling techniques.
Soil organic carbon influences several landscape ecological processes, and soils are becoming recognized as a mechanism to mitigate the negative impacts of climate change. There is a need to define methods and technologies for addressing soils’ spatial variability as well as the time and cost of sampling soil organic carbon (SOC). Visible and near-infrared spectroscopy have been suggested as a sampling tool to reduce inventory cost. We sampled nineteen ranch properties totaling 17,347 ha across Oklahoma and Texas in 2019 to evaluate the effectiveness and accuracy of a handheld reflectometer (Our Sci, Ann Arbor, MI, USA) (370–940 nm) and existing remote sensing approaches to estimate SOC in semi-arid grazing lands. Our data suggest that the Our Sci Reflectometer estimated soil organic carbon with a precision of approximately (±0.3% SOC); however, it was least accurate at higher carbon concentrations. The Our Sci reflectometer, although consistently accurate at lower SOC concentrations, was still less accurate than a model built using only remote sensing and digital soil map data as predictors. Combining the two data sources was the most accurate means of determining SOC. Our results indicated that the Our Sci handheld Vis-NIR reflectometer tested may have only limited applications for reducing inventory costs at scale.
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