This study developed an energy-enhanced (ee)-micro-electric discharge machining (EDM) system for preparing nano-tungsten (nano-W) colloids. This system enables spark discharge using tungsten wires immersed in deionized water, to produce nano-W colloids. Compared with the chemical preparation method, the processing environment for preparing colloids in this study prevented nanoparticle escape. Among the nano-W colloids prepared using the ee-micro-EDM system and an industrial EDM system, the colloid prepared by the ee-micro-EDM system exhibited a more favorable absorbance, suspensibility, and particle size. The colloid prepared by the ee-micro-EDM system with a pulse on time and off time of 10–10 μs had an absorbance of 0.277 at a wavelength of 315 nm, ζ potential of −64.9 mV, and an average particle size of 164.9 nm. Transmission electron microscope imaging revealed a minimum particle size of approximately 11 nm, and the X-ray diffractometer spectrum verified that the colloid contained only W2.00 and W nanoparticles. Relative to industrial EDM applications for nano-W colloid preparation, the ee-micro-EDM system boasts a lower cost and smaller size, and produces nano-W colloids with superior performance. These advantages contribute to the competitiveness of the electrical spark discharge method in the preparation of high-quality nano-W colloids.
This study enhanced the discharge energy of an existing micro-electric discharge machining (EDM) system to provide the system with the ability to prepare nano-tungsten (nano-W) colloid. The energy- enhanced EDM system, referred to as the upgraded-micro-EDM system, enables spark discharge using tungsten wires immersed in deionized water to produce nano-W colloids. Compared with the chemical preparation method, the processing environment for preparing colloids will not have nanoparticle escape in this study. Among the nano-W colloids prepared using the upgraded-micro-EDM system and an industrial EDM system, the colloid prepared by the upgraded-micro-EDM system exhibited more favorable absorbance, suspensibility, and particle size. The colloid prepared by the upgraded-micro-EDM system with the pulse on time and off time of 10–10 µs had an absorbance of 0.277 at the wavelength of 315 nm, ζ potential of −64.9 mV, and an average particle size of 164.9 nm. Transmission electron microscope imaging revealed the minimum particle size of approximately 11 nm, and the X-ray diffractometer spectrum verified that the colloid contained only \({\text{W}}_{2.00}\) and W nanoparticles. Relative to industrial EDM applications for nano-W colloid preparation, the upgraded system boasts lower costs and smaller size, and produces nano-W colloid with superior performance. These advantages contribute to the competitiveness of electrical spark discharge method in the preparation of high-quality nano-W colloids.
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