In this work, the authors present the possibility of characterization of the fracture toughness in mode I (KIC) for TiB2 and TiB2 coatings doped with different concentration of W (3%, 6% and 10%). The Young’s modulus, hardness and fracture toughness of this coatings are extracted from nanoindentation experiments. The fracture toughness was evaluated using calculation of crack length measurement. An important observation is that increasing tungsten concentration in the range 0–10% changes the microstructure of the investigated coatings: from columnar structure for TiB2 coating to nano-composite structure for Ti-B-W (10%) coating. It can be concluded that doping with concentration 10 at.% W causes an increase of the fracture toughness for the tested coatings.
In this work, the authors present the possibility of modification of polymer membranes by TiO2 + AgO coating created by the magnetron sputtering method. The two-component TiO2 + AgO coating can improve and shape new functional properties such as bactericidal and photocatalytic properties. The influence of magnetron power changes on the structure of the membrane was investigated as well. The structure and elemental composition of TiO2 + AgO coatings were analyzed using SEM and EDS technique. All deposited coatings caused a total inhibition of the growth of two investigated colonies of Escherichia coli and Bacillus subtilis on the surface. The photocatalytic properties for membranes covered with oxide coatings were tested under UV irradiation and visible light. The filtration result show that polymer membranes covered with two-component TiO2 + AgO coatings have a permeate flux similar to the non-coated membranes.
Microfiltration (MF) membranes have been widely used for the separation and concentration of various components in food processing, biotechnology and wastewater treatment. The deposition of components from the feed solution and accumulation of bacteria on the surface and in the membrane matrix greatly reduce the effectiveness of MF. This is due to a decrease in the separation efficiency of the membrane, which contributes to a significant increase in operating costs and the cost of exploitative parts. In recent years, significant interest has arisen in the field of membrane modifications to make their surfaces resistant to the deposition of components from the feed solution and the accumulation of bacteria. The aim of this work was to develop appropriate process parameters for the plasma surface deposition of silver oxide (AgO) on MF polyamide membranes, which enables the fabrication of filtration materials with high permeability and antibacterial properties.
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