Bismuth vanadate (Bi2VO5.5) powder has been successfully prepared by microwave method. Bismuth nitrate and ammonium vanadate were used as the starting precursors with the mole ratio of 2:1 in 2-propanol. The microwave power was 500 Watt for 2-6 min. The yellow powder was obtained and calcined at 500°C for 2h. The structure was identified by X-ray diffraction (XRD). The morphology was investigated by scanning electron microscopy (SEM). The chemical composition was determined by energy dispersive X-ray spectrometry (EDXS). The functional groups were investigated by fourier transform infrared spectrometry (FTIR) The photocatalytic degradation of methylene blue (MB) using Bi2VO5.5 powder was studied by ultraviolet-visible spectrophotometry (UV-Vis).
Graphene oxide (GO) powder was synthesized by modified Hummer’s method. Bismuth vanadate (BiVO4) nanoparticle was synthesized by solvothermal method at 100 and 200°C for 3h. Composite graphene oxide and bismuth vanadate (GO/BiVO4) nanoparticle were synthesized by mixed oxide method in weight ratio of 0.20:1.00. The physical and chemical properties were characterized by X-ray diffractometer (XRD), scanning electron microscope (SEM), energy dispersive X-ray spectrometer (EDS) and surface area analyzer (BET). The photocatalytic degradation of methomyl performance was determined by high performance liquid chromatograph (HPLC). Composite GO/BiVO4 nanoparticle at 200°C for 3h was the highest photocatalytic degradation of methomyl.
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