Cobalt oxide nanostructure materials have been prepared by adding several concentrations of spectator Ni ions in solution, and analyzed by electron microscopy, X-day diffraction, calorimetry/thermogravimetric analysis, UV-vis absorption, Raman, and X-ray photoelectron spectroscopy. The electron microscopy results show that the morphology of the nanostructures is dramatically altered by changing the concentration of spectator ions. The bulk XRD patterns of 350 ºC-annealed samples indicate that the structure of the cobalt oxide is all of cubic Fd-3m Co 3 O 4 , and show that the major XRD peaks shift slightly with the concentration of Ni ions. In Raman spectroscopy, we can confirm the XRD data through a more obvious change in peak position, broadness, and intensity. For the un-sputtered samples in the XPS measurement process, the XPS peaks of Co 2p and O 1s for the samples prepared without Ni ions exhibit higher binding energies than those for the sample prepared with Ni ions. Upon Ar + ion sputtering, we found Co 3 O 4 reduces to CoO, on the basis of XPS data. Our study could be further applied to controlling morphology and surface oxidation state.

The effect of the M-window color mixing bar on the characteristics of color mixing and hot spots in the edge-lit backlight employing red (R), green (G), blue (G) light emitting diodes (LED) were studied in terms of the structure of the M-window color mixing bar. The rays from RGB LEDs entering the M-window bar were mixed by internal reflection and scattering inside the M-window bar so that the hot spots and color separation were minimized. The M-window bar was designed and fabricated and the simulation results are matched quite well to experimental data.

This study reports the ZnS quantum dots (QDs) synthesis by a hot-injection method for acetone gas sensing applications. The prepared ZnS QDs were characterized by X-ray diffraction (XRD) and transmission electron microscopy analysis. The XRD result confirms the successful formation of the wurtzite phase of ZnS, with a size of ~5 nm. Transmission electron microscopy (TEM), high-resolution TEM (HRTEM), and fast Fourier transform (FFT) images reveal the synthesis of agglomerated ZnS QDs with different sizes, with lattice spacing (0.31 nm) corresponding to (111) lattice plane. The ZnS QDs sensor reveals a high sensitivity (92.4%) and fast response and recovery time (5.5 s and 6.7 s, respectively) for 100 ppm acetone at 175 °C. In addition, the ZnS QDs sensor elucidates high acetone selectivity of 91.1% as compared with other intrusive gases such as ammonia (16.0%), toluene (21.1%), ethanol (26.3%), butanol (11.2%), formaldehyde (9.6%), isopropanol (22.3%), and benzene (18.7%) for 100 ppm acetone concentration at 175 °C. Furthermore, it depicts outstanding stability (89.1%) during thirty days, with five day intervals, for 100 ppm at an operating temperature of 175 °C. In addition, the ZnS QDs acetone sensor elucidates a theoretical detection limit of ~1.2 ppm at 175 °C. Therefore, ZnS QDs can be a promising and quick traceable sensor nanomaterial for acetone sensing applications.

We developed novel substrate adhesion technique using thermosetting resin to apply roll‐to‐roll process to manufacturing of LCDs. We can use one‐drop‐filling (ODF) process without any distortion of LC alignment using the mixture of thermosetting resin and tetrahydrofuran(THF). This technique can be used to roll‐to‐roll process for flexible LCDs.

Self-aligning Characteristics of Optical Sheets with Apertures (Received September 14, 2009; Revised manuscript October 6, 2009; Accepted October 6, 2009) Optical sheets with apertures on the opposite side of the substrate are designed and analyzed in order to use them as high efficiency light concentration sheets in LCD edge-lit backlight. Formation of apertures by self-aligning exposure were analyzed for the microlens array sheet, pyramid array sheet, and cone array sheet and the microlens array sheet showed the best performance for the formation of apertures by the self-aligning exposure.