The increasing demand for high-strength lightweight concrete (HSLWC) with excellent mechanical properties has inspired the development of nanomaterials in fundamentally solving brittleness and cracking. This work investigated the effects of graphene oxide (GO) on the mechanical properties and microstructure of HSLWC, including the workability, density, compressive strength in different curing regimes, splitting tensile strength, flexural strength, modulus of elasticity and scanning electron microscopy (SEM). Six groups of mixtures were mixed with GO aqueous solution at a dosage of 0.00%, 0.02%, 0.04%, 0.05%, 0.06%, and 0.08% by weight of cement, respectively, and dispersed by ultrasound for 30 min. The test results showed that adding a low volume of GO to the specimens could slightly increase the density, rationally reduce the slump, and significantly improve the mechanical properties. The maximum increase in compressive strength, splitting tensile strength, modulus of elasticity and flexural strength of HSLWC with GO at 28 days was by 24%, 17%, 15%, 20%, respectively, as compared with HSLWC without GO. Simultaneously, the SEM results showed that GO could not only fill nano-scale pores, but also regulate the formation and growth of flower-like crystals, which was an important factor for the further improvement of properties. The research results provided a potential new pathway to improve the mechanical properties of HSLWC.

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An effective pathway to achieve the sustainable development of resources and environmental protection is to utilize shale ceramsite (SC), which is processed from shale spoil to produce high-strength lightweight concrete (HSLWC). Furthermore, the urgent demand for better performance of HSLWC has stimulated active research on graphene oxide (GO) in strengthening mechanical properties and durability. This study was an effort to investigate the effect of different contents of GO on HSLWC manufactured from SC. For this purpose, six mixtures containing GO in the range of 0–0.08% (by weight of cement) were systematically designed to test the mechanical properties (compressive strength, flexural strength, and splitting tensile strength), durability (chloride penetration resistance, freezing–thawing resistance, and sulfate attack resistance), and microstructure. The experimental results showed that the optimum amount of 0.05% GO can maximize the compressive strength, flexural strength, and splitting tensile strength by 20.1%, 34.3%, and 24.2%, respectively, and exhibited excellent chloride penetration resistance, freezing–thawing resistance, and sulfate attack resistance. Note that when the addition of GO was relatively high, the performance improvement in HSLWC as attenuated instead. Therefore, based on the comprehensive analysis of microstructure, the optimal addition level of GO to achieve the best mechanical properties and durability of HSLWC is considered to be 0.05%. These findings can provide a new method for the use of SC in engineering.