Roughness-induced closure is held to be responsible for very low fatigue crack growth rates observed in certain plate orientations of Al-Li 2090 T8E41, and the geometry of asperities producing this closure correlates with macrotexture. Little work, however, has focused on the role of individual grain orientations (microtexture) or of average orientation within small groups of adjacent grains (mesotexture) on the crack's path through a sample, i.e., on whether the variation in grains' orientations determines where the crack will deflect. This paper reports synchrotron X-ray microbeam diffraction mapping of the three-dimensional microtexture in samples of Al-Li 2090. Groups of adjacent pancake-shaped grains are found to have very similar orientations, producing nearly single-crystal regions approaching thicknesses of 0.3 mm along the sample's S (short-transverse) direction. These near-single-crystal volumes produce large asperities with surfaces having substantial Mode III character, asperities which appear over the range of stress intensity ranges observed (∼5 to ∼25 MPa√m). Results of these experiments suggest not only that this type of mesotexture plays an important role in determining fatigue crack path in compact tension samples of Al-Li 2090 but also that specific orientations of the groups of grains lead to large crack deflections.
A weight loss rate-controlled organic extraction furnace was built and demonstrated using a multilayer green ceramic. Multirate weight loss schedules as well as automated atmosphere control and detection were demonstrated. The low thermal mass furnace showed good tracking with 300 °C heating and cooling rates. This furnace, coupled with appropriate PID control constants, facilitated feedback control which could extract organics rapidly without self-ignition to uncontrolled combustion. Controlled organic burnout was demonstrated at weight loss rates up to 0.5%/min in air. Damage-free multilayers were observed using a burnout rate requiring 150 min for extraction, rather than the days commonly associated with this task when using conventional furnaces.
The use of synchrotron polychromatic x-ray microbeams in the transmission geometry is described for mapping grain orientation as a function of position and for relating this microtexture to the formation of large asperities on fatigue crack surfaces in Al-Li 2090 T8E41. In common with the centers of rolled plates of many aluminum alloys, Al-Li 2090 T8E41 has a sharp average texture or macrotexture different from that in the outer portions of the plate. The geometry of large asperities in Al-Li 2090 has been related to this macrotexture, and the resulting roughness-induced crack closure is recognized to be responsible for the very low crack propagation rates in certain plate orientations. This report focuses on why asperities form at certain positions and why the crack remains relatively planar elsewhere. The microtexture (i.e., the grain-to-grain orientation variation) seems to be organized into a specific type of mesotexture: multiple adjacent grains have nearly identical orientations and form substantial volumes of near-single-crystal material. Transitions between differently oriented near-singlecrystal volumes or between a near-single- crystal region and more randomly oriented grains appear to bound asperities.
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