PrecIPItatIon Processes durIng non-Isothermal ageIng of fIne-graIned 2024 alloyMechanical alloying and powder metallurgy procedures were used to manufacture very fine-grained bulk material made from chips of the 2024 aluminum alloy. Studies of solution treatment and precipitation hardening of as-received material were based on differential scanning calorimetry (DSC) tests and TEM/STEM/EDX structural observations. Structural observations complemented by literature data lead to the conclusion that in the case of highly refined structure of commercial 2024 alloys prepared by severe plastic deformation, typical multi-step G-P-B →θ" →θ' →θ precipitation mechanism accompanied with G-P-B →S" →S' →S precipitation sequences result in skipping the formation of metastable phases and direct growth of the stable phases. Exothermic effects on DSC characteristics, which are reported for precipitation sequences in commercial materials, were found to be reduced with increased milling time. Moreover, prolonged milling of 2024 chips was found to shift the exothermic peak to lower temperature with respect to the material produced by means of common metallurgy methods. This effect was concluded to result from preferred heterogeneous nucleation of particles at subboundaries and grain boundaries, enhanced by the boundary diffusion in highly refined structures.Transmission electron microscopy and diffraction pattern analysis revealed the development of very fine Al4C3 particles that grow due to the chemical reaction between the Al matrix and graphite flakes introduced as a process control agent during the preliminary milling of chips. Al4C3 nano-particles are formed at high temperatures, i.e. during hot extrusion and the subsequent solution treatment of the samples. Highly refined insoluble particles such as aluminum carbide particles and aluminum oxides were found to retard recrystallization and reduce recovery processes during solution treatment of preliminarily milled materials. Therefore, the as-extruded material composed of a milled part and chip residuals retained its initial bimodal structure in spite of solution heat treatment procedures. This points to a high structural stability of the investigated materials, which is commonly required for new technologies of high-strength Al-based materials production.
In the study microstructure and properties of composite multifibre copper-base wires are presented. A decision was made to produce wires with "soft" fibres (Al) and "hard" fibres (Fe). In the study the phenomenon occurring on the border of Al-Cu was also analysed. The produced Cu-Al and Cu-Fe composites presented ordered microstructure with the fibres uniformly distributed in the copper matrix. The composites underwent plastic consolidation to the degree which provided satisfactory mechanical and electrical properties. During the drawing the fibres deformed proportionally with copper matrix therefore their content in the cross section remained unchanged.
The aim of this work was to study the microstructure and mechanical properties of copper, brass CuZn36 and bronze CuSn6 strips annealed and after repetitive corrugation and straightening (RCS) process. The influence of process parameters on the functional properties of strips was investigated. The study found an increase in the yield strength and tensile strength of the material after RCS process. Crystallite size measurement confirmed the presence of nanoscale structures in the studied materials after deformation by RCS process. The used method of plastic deformation is promising for development materials with improved functional properties. The paper presents also the results of numerical simulations of Cu strip after corrugation on groove and tooth rolls and next straightening. Rolling process simulations were conducted using Forge 2011® based on the finite element method.
The required functional characteristics expected from copper alloys have a major impact on the technological production process, therefore there is a strong need to acquire knowledge on changes of properties with technological process including heat treatment and plastic working. The studied in this work copper CuTi4. CuFe2. CuCr0.7 and CuNi2Si1 alloys was selected to present differences in hardening phases .The samples were quenched, cold deformed (rolling), and aged. Detailed microstructure analysis and its influence on electrical and mechanical properties was presented in the work. Quenched CuTi4, CuFe2, CuCr0.7 and CuNi2Si1alloys have different mechanism and kinetics of precipitation during aging. These processes are complex and depend on the heterogeneity of distribution of alloying elements in copper matrix, the process parameters and cold strain value.Keywords: hardened copper alloys, mechanical properties, electrical conductivity, microstructureWymagane cechy użytkowe których oczekuje się od stopów miedzi wywierają zasadniczy wpływ na ich technologiczny proces wytwarzania. Wynika stąd konieczność rozeznania zakresu zmian własności użytkowych wynikających z zastosowanego wariantu obróbki cieplnej i plastycznej. Stopy miedzi CuTi4, CuFe2, CuCr0.7 i CuNi2Si1 poddane badaniu w niniejszej pracy dobrano w ten sposób aby różniły się fazami umacniającymi. Próbki poddano przesycaniu, odkształceniu na zimno (walcowanie) oraz starzeniu. Przesycone stopy CuTi4, CuFe2, CuCr0.7 oraz CuNi2Si1 różnią się mechanizmem i kinetyką wydzielania podczas procesu starzenia. Procesy te są złożone i uzależnione od niejednorodności rozmieszczenia składników stopowych w osnowie miedzianej, historii wytwarzania i przetwarzania stopów, parametrów przesycania i starzenia jak tez wielkości odkształcenia na zimno.
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