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This work deals with the examination of the mechanical properties of Aluminium (LM6) reinforced with iron oxide (Fe2O3). Stir casting process is used to formulate the composite sampling by varying iron oxide in 5% and 10% by weight. Three different heat treatment process of hardening, annealing and normalizing is carried out on samples of aluminium (LM6), aluminium (LM6) + 5% Fe2O3 and aluminium (LM6) + 10% Fe2O3. Composite specimens are tested to analyze the mechanical properties such as hardness, yield stress, tensile strength and elongation. Present reinforcement specks enabled the alloy to preserve higher hardness during the heat treatment. Results have shown substantial improvements in properties of the specimens with various compositions of reinforcement.