Using an optimally coupled nanometer-scale SQUID, we measure the magnetic flux originating from an individual ferromagnetic Ni nanotube attached to a Si cantilever. At the same time, we detect the nanotube's volume magnetization using torque magnetometry. We observe both the predicted reversible and irreversible reversal processes. A detailed comparison with micromagnetic simulations suggests that vortexlike states are formed in different segments of the individual nanotube. Such stray-field free states are interesting for memory applications and noninvasive sensing.
We experimentally demonstrate the occurrence of negative absolute resistance (NAR) up to about −1Ω in response to an externally applied dc current for a shunted Nb-Al/AlOx-Nb Josephson junction, exposed to a microwave current at frequencies in the GHz range. The realization (or not) of NAR depends crucially on the amplitude of the applied microwave current. Theoretically, the system is described by means of the resistively and capacitively shunted junction model in terms of a moderately damped, classical Brownian particle dynamics in a one-dimensional potential. We find excellent agreement of the experimental results with numerical simulations of the model.
Superconductivity in the cuprate YBa(2)Cu(3)O(7) (YBCO) persists up to huge magnetic fields (B) up to several tens of Teslas, and sensitive direct current (dc) superconducting quantum interference devices (SQUIDs) can be realized in epitaxially grown YBCO films by using grain boundary Josephson junctions (GBJs). Here we present the realization of high-quality YBCO nanoSQUIDs, patterned by focused ion beam milling. We demonstrate low-noise performance of such a SQUID up to B = 1 T applied parallel to the plane of the SQUID loop at the temperature T = 4.2 K. The GBJs are shunted by a thin Au layer to provide nonhysteretic current voltage characteristics, and the SQUID incorporates a 90 nm wide constriction which is used for on-chip modulation of the magnetic flux through the SQUID loop. The white flux noise of the device increases only slightly from 1.3 μΦ(0)/(Hz)(1/2) at B = 0 to 2.3 μΦ(0)/(Hz))(1/2) at 1 T. Assuming that a point-like magnetic particle with magnetization in the plane of the SQUID loop is placed directly on top of the constriction and taking into account the geometry of the SQUID, we calculate a spin sensitivity S(μ)(1/2) = 62 μ(B)/(Hz))(1/2) at B = 0 and 110 μ(B)/(Hz))(1/2) at 1 T. The demonstration of low noise of such a SQUID in Tesla fields is a decisive step toward utilizing the full potential of ultrasensitive nanoSQUIDs for direct measurements of magnetic hysteresis curves of magnetic nanoparticles and molecular magnets.
We investigated, at temperature 4.2 K, electric transport, flux noise and resulting spin sensitivity of miniaturized Nb direct current superconducting quantum interference devices (SQUIDs) based on submicron Josephson junctions with HfTi barriers. The SQUIDs are either of the magnetometertype or gradiometric in layout. In the white noise regime, for the best magnetometer we obtain a flux noise S 1/2 Φ = 250 nΦ0/Hz 1/2 , corresponding to a spin sensitivity S 1/2 µ ≥ 29 µB/Hz 1/2 . For the gradiometer we find S 1/2 Φ = 300 nΦ0/Hz 1/2 and S 1/2 µ ≥ 44 µB/Hz 1/2 . The devices can still be optimized with respect to flux noise and coupling between a magnetic particle and the SQUID, leaving room for further improvement towards single spin resolution.
YBa 2 Cu 3 O 7 24 • (30 •) bicrystal grain boundary junctions (GBJs), shunted with 60 nm (20 nm) thick Au, were fabricated by focused ion beam milling with widths 80 nm w 7.8 μm. At 4.2 K we find critical current densities j c in the 10 5 A cm −2 range (without a clear dependence on w) and an increase in resistance times junction area ρ n with an approximate scaling ρ n ∝ w 1/2. For the narrowest GBJs j c ρ n = I c R n ≈ 100 μV (with critical current I c and junction resistance R n), which is promising for the realization of sensitive nanoSQUIDs for the detection of small spin systems. We demonstrate that our fabrication process allows the realization of sensitive nanoscale dc SQUIDs; for a SQUID with w ≈ 100 nm wide GBJs we find an rms magnetic flux noise spectral density of S 1/2 ≈ 4 μ 0 Hz −1/2 in the white noise limit. We also derive an expression for the spin sensitivity S 1/2 μ , which depends on S 1/2 , on the location and orientation of the magnetic moment of a magnetic particle to be detected by the SQUID, and on the SQUID geometry. For the unoptimized SQUIDs presented here, we estimate S 1/2 μ = 390 μ B Hz −1/2 , which could be further improved by at least an order of magnitude.
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