Sol-gel method is the simplest method and has the ability to control the particle size and morphology through systematic monitoring of reaction parameters. The objective of this research is to synthesize silica nanostructures by sol-gel method and to characterize the synthesized silica nanostructures. Silica nanoparticles were synthesized via the sol-gel method using Tetraethyl orthosilicate as a precursor. The acetic acid and distilled water were used as the catalyst and the hydrolyzing agent. Varied parameters of the study were the aging time in the range of 2 to 6 h and the calcination temperature in the range of 600-700• C. The obtained silica nanopowder was characterized using FESEM, and Nano-Particle Size Analyzer. The results show that the silica nanospheres were successfully synthesized by using sol-gel method with the optimum parameters of 700• C of calcination temperature and 2 h of aging time. The average size of silica nanoparticles was in the range of 79.68 nm to 87.35 nm.
Nanostructured coatings offer great potential for various applications due to their superior characteristics that are not typically found in conventional coatings. This research aimed at developing a new and improved coating that employs zinc oxide nanopowder as the agent to achieve corrosion resistant properties for a coating. The research project discusses on its corrosion behaviour of epoxy-zinc oxide in different media by measuring its corrosion rate. Mild carbon steel was used as the substrate for the epoxy-zinc oxide coating. The corrosion behavior mechanism of mild steel was investigated in different media, namely fresh water, NaCl solution, HCl solution and NaOH solution. Immersion test was conducted and studied for a period of 60 days, with daily and weekly weighing and immersing. The corrosion rate was calculated and mild steel corrodes in the different environment and degrades in the following trend; HCl → NaCl → NaOH → H2O.
Nanocoating acted as a barrier to avoid the transportation of corrosive species. Nanoparticles provide the resin or coating with a continuous, solid and protective network layer. Silicon wafer p-type substrate <101> was used as standard materials while tungsten wire of 0.15mm diameter was used as tip for scanning operation. Nanoeducator showed that present of nanoparticles increase the surface roughness and maintain the size of nanoparticles. Nanoparticles well distribute in nanosize. Immersion test showed nanoparticles also, improved the adherence of the cured epoxy coating.
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