The wide scale use of small specimens in routine testing programs could significantly reduce material resource requirements (factors of 10 are easily achievable). This is a major benefit to situations where there is not enough material to manufacture conventional, full-size specimens, such as first-stage gas turbine blade roots. However, limitations exist due to concerns over size effects, manufacturing difficulties, uncertainties related to the application of representative loading conditions and complex interpretation procedures of non-standard data. Due to these limitations, small specimen testing techniques have been mostly applied in ranking exercises and to determine approximate or simple material parameters such as Young's modulus, minimum creep strain rate and fracture toughness. The small ring method is a novel, high sensitivity small specimen technique for creep testing that has been extended in the present work to the determination of tensile material properties. The main advantages of the small ring specimen are that it is self-aligning and has a large equivalent gauge length in comparison to other small specimens, resulting in much higher testing sensitivity. In the present work, this specimen type mimics conventional, full-size, monotonic testing, allowing for observations of elastic and plastic material response to be made. Wrought aluminium alloy 7175-T7153 small rings were tested at room temperature at 5 different loading (displacement) rates and the results compared to conventional, full-size, monotonic specimen equivalents. Finite element analysis was conducted in order to evaluate the equivalent gauge section and equivalent gauge length in the small ring specimen (which varied between circa 0.35-1.4mm 2 and 25-45mm, respectively) to facilitate these comparisons. An analytical solution has also been derived in order to validate the finite element analysis.

Small specimen mechanical testing is an exciting and rapidly developing field in which fundamental deformation behaviours can be observed from experiments performed on comparatively small amounts of material. These methods are particularly useful when there is limited source material to facilitate a sufficient number of standard specimen tests, if any at all. Such situations include the development of new materials or when performing routine maintenance/inspection studies of in-service components, requiring that material conditions are updated with service exposure. The potentially more challenging loading conditions and complex stress states experienced by small specimens, in comparison with standard specimen geometries, has led to a tendency for these methods to be used in ranking studies rather than for fundamental material parameter determination. Classifying a specimen as ‘small’ can be subjective, and in the present work the focus is to review testing methods that utilise specimens with characteristic dimensions of less than 50 mm. By doing this, observations made here will be relevant to industrial service monitoring problems, wherein small samples of material are extracted and tested from operational components in such a way that structural integrity is not compromised. Whilst recently the majority of small specimen test techniques development have focused on the determination of creep behaviour/properties as well as sub-size tensile testing, attention is given here to small specimen testing methods for determining specific tensile, fatigue, fracture and crack growth properties. These areas are currently underrepresented in published reviews. The suitability of specimens and methods is discussed here, along with associated advantages and disadvantages.

The use of small specimens in routine testing would reduce resource requirements, however, limitations exist due to concerns over size effects, manufacturing difficulties, uncertainties related to the application of representative loading conditions, and complex interpretation procedures of non-standard data. Due to these limitations, small specimen testing techniques have been mostly applied for ranking exercises and to determine approximate or simple material parameters such as Young's modulus, creep minimum strain rate and fracture toughness. The small ring method is a novel, high sensitivity small specimen technique for creep testing and has been extended in the present work for the determination of tensile material properties. Wrought aluminium alloy 7175-T7153 was tested at room temperature at 5 different loading rates. Finite element analysis was completed to evaluate the equivalent gauge section and equivalent gauge length in order to compare uniaxial tensile testing results and small ring specimen tensile testing results. An analytical solution has also been derived in order to validate the finite element analysis. It was discovered that the finite element analysis model was suitable, validated by both experimental results and analytical solution as well as that small ring specimens can be used to acquire same stress/strain data as uniaxial specimens.

Thermo-mechanical coupling is a critical component in the thermodynamics of irreversible processes and is related to the dissipation of thermal energy during plastic straining. The Taylor-Quinney coefficient may be thought of as a ratio between thermally dissipated energy and plastic work, thereby giving insight into the thermomechanical coupling term. The inclusion of this parameter in a meaningful way is complicated by the various dependencies that the Taylor-Quinney coefficient may be subject to (e.g. loading rate and temperature). Determination of these dependencies is usually achieved through extensive experimentation, wherein temperature variations are monitored (with reference to an unloaded control sample) in a test piece during mechanical loading. There are practical limitations in full size testing methods however, not least relating to the location of full sized control and loaded samples in an environment chamber/furnace while simultaneously maintaining (control sample) temperature uniformity and high resolution temperature measurement (in the loaded sample). The present work details a method based on a novel small specimen testing technique that is currently under development at the University of Nottingham. A small ring of 7175-T7351 aluminum alloy (approximately 10mm in diameter and 2mm in thickness) is loaded between two pins at room temperature, with the local specimen temperature field monitored during monotonic deformation using an infra-red thermal camera. Experimental results are compared for different pin loading rates (namely 0.1mm/s, 1mm/s, and 10mm/s), with particular emphasis placed on localised temperature variations in areas of expected high plasticity. Differences of approximately 0.6°C were observed between 0.1mm/s and 1mm/s tests, with higher temperatures recorded in the latter. Higher temperatures were also noted at small specimen locations associated with localised plasticity. Fundamental thermal material properties are reported for the 7175 alloy in order to facilitate future analysis and heat equation solution efforts (working towards Taylor-Quinney coefficient determination).

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