The accelerator mass spectrometry (AMS) center at Horia Hulubei National Institute for R&D in Physics and Nuclear Engineering, Bucharest, is based on the latest-generation 1 MV Tandetron® accelerator, produced by High Voltage Engineering Europa (HVEE), The Netherlands. The AMS center became fully functional at the start of 2013, and at the end of 2015 the laboratory established the RoAMS international code and it was added to the list of AMS laboratories maintained by Radiocarbon journal. An important aspect in the establishment of a new AMS laboratory is the declaration and documentation of the adopted protocols and to demonstrate the reliability and reproducibility of the measurements in comparison to internationally recognized reference materials. In this paper, we present the dating results on the Sixth International Radiocarbon Intercomparison (SIRI) samples that were pretreated, graphitized, and measured in our laboratory. The newly developed sample preparation laboratory can handle sample materials as (1) organic materials, (2) wood, (3) bones, and (4) carbonates. The results of our measurements are in very good agreement with the SIRI consensus values and confirm the reliability of our sample preparation laboratory and also the good performance of the HVEE AMS system. The blank levels for the SIRI materials are 0.277±0.045/0.333±0.046 percent modern carbon (pMC) for wood samples, 0.441±0.038 pMC for bone collagen, and 0.239±0.030 pMC for carbonate materials, considering an average mass of 1 mg sample graphite.
For the ultrasensitive determination of 244Pu by Accelerator Mass Spectrometry, a suitable methodology was developed at the IFIN-HH AMS laboratory. Alpha Spectrometry was used to verify the performance of the...
The aim is to introduce and characterize a new experimental demonstrative model contributing to the increase of measurement accuracy, in terms of minimum detectable activity (MDA) and background reduction, for the analysis of samples having low concentrations in tritium and radiocarbon on Quantulus 1220. The clue is related to the qualitative and quantitative differences between tritium and carbon‐14 inventories of the pulp used to manufacture the cups involved in noncatalytic combustion of samples by flame oxidation method. The quality of the experimental results depends on the temporal origin of the wood from which the pulp/cellulose was extracted/purified, the specific inventory contributing to the threshold level of the MDA for the beta‐emitting radionuclide to be investigated. Finally, the aim is to create and to use such a 100% old cellulose combustion cups for determining low concentrations of these radionuclides. It may be obtained by an adapted technology following the literature data and may be recommended for routine analyses of environmental samples coming from areas with no nuclear or minor nuclear influences, and also for low‐level biological samples. This first attempt resulted in improvement of measurement performances up to 400% for carbon‐14 and by approximately 50% for tritium.
The preventive archaeological excavations from 2011 made possible the unveiling of a significant part of the archaeological site from Turdaș, Luncă point. Thousands of archaeological features were researched, also the defensive system of the site, the habitation neighborhoods and some other results of the human works (C403 and C1878 features)
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