Ceramic additive manufacturing allows the fabrication of small series of complex parts without the high costs of molds usually associated with traditional ceramic processing. Although research into ceramic 3D printing by all technologies started back in the 90s, its industrial application is still quite restricted when compared to polymers and metals, which is related to the limited availability and costs of equipment and materials for such applications. This review examined the advantages and limitations of each process (binder jetting, direct ink writing, directed energy deposition, fused deposition, material jetting, selective laser sintering, selective laser melting, and vat photopolymerization), discussing their particularities. It also summarized the commercially available 3D printers and raw materials for ceramic processing, pointing out to trends and challenges of each technology.
Vat photopolymerization (VP) stands out among ceramic additive manufacturing processes for its ability to print sub-100 micrometer complex features. One of the main challenges of this process is the preparation of a homogeneous and stable ceramic slurry with a high solid load and low viscosity. In this work, different dispersants and resins were tested, aiming to provide a solvent-free slurry suitable for DLP additive manufacturing. Disperbyk-111 and PEGDA 250 stood out in the tests, providing a 40 vol% ceramic slurry with no noticeable sedimentation and viscosity of 2.3 Pa.s at 30 s -1 despite the relatively high specific surface area (15 m 2 /g) of the 3Y-TZP powder used compared to powders usually used for VP slurries. The adsorption of Disperbyk-111 on ceramic particles surface was investigated by FTIR. Finally, ceramic bodies were 3D printed, debound and sintered at 1500 ºC for 2 h, confirming the ability to manufacture detailed dense ceramic parts.
Additive manufacturing processes have been developed over the last decades, especially vat photopolymerization (VP) processes, due to its simplicity and speed. The objective of this paper is to characterize commercial VP resins widely used for technical applications. Thus, test specimens were printed by Digital Light Processing and subjected to tensile, compression, flexural, hardness, and inorganic composition analyses. The resin with the highest resistance and hardness (containing 0.6 vol% of inorganics load) reached 53 MPa in tension, 110 MPa in compression, 79 MPa in bending, and 82.3 Shore D, which is comparable to injected polymers. A case study was made, replacing the injected gears of a reducer by printed ones and comparing the finite element analysis with resin properties. The characterization and case study results encourage the expansion of VP processes in the manufacturing of products in several industries and service sectors, as well as the development of new composite resins.
The design of modern mechanical components often requires the use of low-density and high-strength parts. Additive manufacturing presents competence in obtaining format complexity internally (voids, ducts, channels) and externally (shape, holes). However, parts obtained by material extrusion additive manufacturing are highly anisotropic and relatively weak. This paper aims to present a new mechanical design technique that combines the high geometry flexibility of additive manufacturing with internal structuring reinforcement by high-strength materials, which enables optimized parts with reinforcement in the most mechanical stressed areas during service, through adopting structured internal geometry filled with reinforcement material. Dense test specimens and test specimens with internal structural canals filled with reinforcement material (epoxy resin and carbon fibers) were designed, fabricated and tested physically and virtually. The obtained results provide property values for 3D-printed acrylonitrile butadiene styrene (typical material of additive manufacturing) and for this polymer reinforced with various reinforcement material configurations (useful for mechanical design). The reinforcement decreased anisotropy and improved mechanical properties. Optimized parts filled with resin and long carbon fibers had maximum flexural resistance of 112 MPa, with a specific weight of 1.1 g/cm3. This reinforcement provided parts with specific flexural strength similar to structural aluminum alloys, preserving the geometry and external dimension of the printed parts. The technique presented here shows the possibility of new conceptions in mechanical components design and strength optimization by internal reinforcement canals in parts. The technique is useful for mechanical design activity and allows for new product conceptions based on additive manufacturing.
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