Asphalt self-healing by encapsulated rejuvenating agents is considered a revolutionary technology for the autonomic crack-healing of aged asphalt pavements. This paper aims to explore the use of Bio-Oil (BO) obtained from liquefied agricultural biomass waste as a bio-based encapsulated rejuvenating agent for self-healing of bituminous materials. Novel BO capsules were synthesized using two simple dripping methods through dropping funnel and syringe pump devices, where the BO agent was microencapsulated by external ionic gelation in a biopolymer matrix of sodium alginate. Size, surface aspect, and elemental composition of the BO capsules were characterized by optical and scanning electron microscopy and energy-dispersive X-ray spectroscopy. Thermal stability and chemical properties of BO capsules and their components were assessed through thermogravimetric analysis (TGA-DTG) and Fourier-Transform Infrared spectroscopy (FTIR-ATR). The mechanical behavior of the capsules was evaluated by compressive and low-load micro-indentation tests. The self-healing efficiency over time of BO as a rejuvenating agent in cracked bitumen samples was quantified by fluorescence microscopy. Main results showed that the BO capsules presented an adequate morphology for the asphalt self-healing application, with good thermal stability and physical-chemical properties. It was also proven that the BO can diffuse in the bitumen reducing the viscosity and consequently self-healing the open microcracks.
Effect of metallic waste addition on the electrical, thermophysical and microwave crackhealing properties of asphalt mixtures Norambuena-Contreras, J.; Gonzalez, A.; Concha, J. L.; Gonzalez-Torre, I.; Schlangen, E. h i g h l i g h t sFibres and shavings from metallic waste were added in asphalt mixtures. Electrical, thermophysical and microwave crack-healing properties of asphalt were evaluated. CT-Scan results showed that shavings were crushed during asphalt mixing process. Metallic waste addition did not improve thermal and electrical properties. Healing levels after microwave heating times of 40 s twice those obtained after 30 s. a b s t r a c tThis paper aims to evaluate the effect of metallic waste addition on the electrical, thermophysical and microwave crack-healing properties of asphalt mixtures. With this purpose, asphalt mixtures with two different types of metallic waste, steel wool fibres and steel shavings, added in four different contents, were tested. Electrical and thermophysical properties of asphalt mixture specimens with, and without, metallic waste were measured. The spatial distribution of the metallic waste inside the asphalt mixture samples was evaluated by using X-ray computed tomography. In addition, crack-healing properties of asphalt samples using microwave radiation heating were assessed at two different healing times, 30 s and 40 s. To quantify the efficiency of the healing process, five healing cycles were carried out for each asphalt sample. The main results showed that asphalt mixtures with shavings presented lower air void contents than mixtures with fibres. Moreover, fibres produced an increase in the electrical conductivity of the mixtures because long fibres in the mixtures form electrically conductive channels. In contrast, shavings did not have significant effect on the electrical properties of the mixtures. Likewise, it was proven that metallic waste reduced the thermal conductivity and the specific heat capacity of asphalt mixtures. Conversely, shavings decreased the thermal diffusivity of asphalt mixtures regardless of their content. Overall, it was found that the healing level reached by the asphalt mixtures tested by microwave radiation depends on the healing time and the type and content of metallic waste used. CT-scans results proved that the spatial distribution of metallic waste inside the asphalt mixture samples was not uniform and played an important role in the asphalt self-healing properties using microwave radiation heating.
Featured Application: A new generation of advanced self-healing asphalt pavements is coming. The asphalt mixture presented in this study could be potentially used to build long-life roads with crack-healing properties through electromagnetic heating, e.g., induction and microwaves.Abstract: This paper aims to evaluate the influence of the microwave heating time on the self-healing properties of fibre-reinforced asphalt mixtures. To this purpose, self-healing properties of dense asphalt mixtures with four different percentages of steel wool fibres were evaluated as the three-point bending strength before and after healing via microwave heating at four different heating times. Furthermore, the thermal behaviour of asphalt mixtures during microwave heating was also evaluated. With the aim of quantifying the efficiency of the repair process, ten damage-healing cycles were done in the test samples. In addition, self-healing results were compared with the fibre spatial distribution inside asphalt samples evaluated by CT-scans. Crack-size change on asphalt samples during healing cycles was also evaluated through optical microscopy. It was found that the heating time is the most influential variable on the healing level reached by the asphalt mixtures tested by microwave radiation. CT-Scans results proved that fibre spatial distribution into the asphalt mixtures play an important role in the asphalt healing level. Finally, it was concluded that 40 s was the optimum heating time to reach the highest healing levels with the lowest damage on the asphalt samples, and that heating times over 30 s can seal the cracks, thus achieving the self-healing of asphalt mixtures via microwave heating.
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