The efficiency of a centrifugal pump for mechanical pump fluid loops, apart from the design, relies on the performance of the closed impeller which is linked to the manufacturing process in terms of dimensional accuracy and the surface quality. Therefore, the activities of this paper were focused on defining the manufacturing process of a closed impeller using the additive manufacturing technology for mechanically pumped fluid loop (MPFL) systems in space applications. Different building orientations were studied to fabricate three closed impellers using selective laser melting technology and were subjected to dimensional accuracy and surface quality evaluations in order to identify the optimal building orientation. The material used for the closed impeller is Inconel 625. The results showed that both geometrical stability and roughness were improved as the building orientation increased, however, the blade thickness presented small deviations, close to imposed values. Finishing processes for inaccessible areas presented significant results in terms of roughness, nevertheless, the process can be further improved. Abrasive flow machining (AFM) post-processing operations have been considered and the results show major improvements in surface quality. Thus, important steps were made towards the development of complex structural components, consequently increasing the technological readiness level of the additive manufacturing process for space applications.
The activities of this paper were focused on an in-situ fabrication process for producing two self-healing systems containing dicyclopentadiene and 5-ethylidene-2-norbornene monomers encapsulated in a urea-formaldehyde shell and integration methods applied in the epoxy matrix to analyse and compare the influences of their integration into the neat epoxy matrix. The self-healing systems were first synthesized according to a literature review, and subsequently, an optimization process was conducted for the fabrication process. Neat epoxy specimens were fabricated as reference specimens and subjected to flexural tests. Several integration methods for incorporating the self-healing systems into the epoxy resin were investigated. The optimal method presenting the best dispersion of the healing system was achieved by reducing the viscosity of the epoxy matrix with 10 vol % acetone solution, the addition of a microcapsule in the matrix, and homogenization at 60 °C at 100 rpm. Thermal analysis was performed in order to observe the mass loss obtained with an increasing temperature and phase changes for both poly-urea-formaldehyde (PUF)-dicyclopentadiene (DCPD) and melamine-urea-formaldehyde (MUF)-5-ethylidene-2-norbornene (ENB) systems. The thermogravimetric analysis performed for the PUF-DCPD system indicates a total loss of mass in the range of 30–500 °C of 72.604% and for the MUF-ENB system, indicates a total mass loss in the range of 30–500 °C of 74.093%. Three-point bending tests showed higher mechanical properties for PUF-DCPD (80%) than MUF-ENB (40%) compared to the neat epoxy systems. Numerical simulations were performed to obtain a better understanding of the microcapsule behavior when embedded in an epoxy matrix.
Nowadays scientific researchers aim to develop new material designs for space structures that can withstand the harsh conditions in space environment. Another goal is to reduce the weight and the launching cost of the structures. A solution to those needs is to integrate fiber reinforced polymers in spacecraft structural components. Radiation shielding is a requirement that has to be met by the materials used to manufacture space structures. Protons are one of the many charged particles that can influence the integrity of materials in space. In the present study three material designs were developed and their ability to shield proton beam irradiation was evaluated. The material designs consist in advanced composite materials (carbon fiber reinforced polymers - CFRPs) that integrate the concept Low Z - High Z - Low Z (tantalum foil) and metallic coatings. Simulations were performed to determine the penetration depth of an ion beam (energy 15 MeV) in the proposed material designs. It was observed that the beam�s penetration depth through a CFRP sample with Ta foil (sample�s thickness 2.08 mm) was about 75% of the sample�s thickness, 58% for CFRP sample with Babbitt coating (sample�s thickness 2.28 mm), 56% for the CFRP sample with Zn coating (sample�s thickness 2.28 mm) and 55% for the CFRP sample with Zn/Monel coating (sample�s thickness 2.28 mm). It seems that the proposed material designs provide ion beam protection similar with an aluminum sample of 2 mm thickness. The experimental procedure confirmed the results obtained from the simulations, all the material designs providing protection in case of proton beam irradiation with an energy of 15.8 MeV.
The present paper is focused on evaluating the mechanical characterization of dicyclopentadiene (DCPD) and 5-ethylidene-2-norbornene (ENB) healing systems synthetized by in-situ polymerisation. Both healing systems were embedded in glass fibre reinforced polymer (GFRP) composite and subjected to three-point bending test regime. Microstructural and FT-IR analysis showed the formation of microcapsules and a successful integration in the composite material. To observe the influence of temperature variation, some specimens were exposed to thermal cycling (-20oC to +100oC) for 12 hours and tested in the same conditions. It was observed that the addition of microcapsules in the composite material decreased its mechanical properties by 8% and 10% for DCPD system and ENB system respectively. Thermal cycling suggested a drop of 24% on bending strength for DCPD system and 17% for ENB. Resting after 24 hours showed a healing recovery of 74% for DCPD healing system and of 97% for ENB system.
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