The crystal and magnetic structures of van der Waals layered ferromagnet CrBr3 were studied using X-ray powder diffraction and neutron powder diffraction at pressures up to 23 GPa at ambient temperature and up to 2.8 GPa in the temperature range 6–300 K, respectively. The vibration spectra of CrBr3 were studied using Raman spectroscopy at pressures up to 23 GPa at ambient temperature. The anomalous pressure behavior of structural parameters and vibrational modes was observed, associated with a gradual isostructural phase transition in the pressure range 2.5–7 GPa. The Curie temperature TC reduced rapidly with a pressure coefficient dTC/dP=−4.1(4) K/GPa. A full suppression of the ferromagnetic state was expected at PC~8.4 GPa, where onset of the antiferromagnetic spin arrangement or magnetically disordered state may take place. Anomalies in Raman spectra at P~15 GPa point to another possible phase transformation in CrBr3, which may be related to the proximity of metallization of this van der Waals ferromagnet.
Volumetric studies of mica spatial distribution inside samples of Westerly and Czech granites (Mrakotin, Liberec, and Brno syenite) were performed using a neutron tomography method. A significant difference in the neutron attenuation coefficients of mica and other rock-forming minerals of the granites studied yielded a large neutron radiography contrast and, as a result, allowed us to perform a detailed analysis of three-dimension structural data based on the neutron tomography reconstruction procedure. The morphology and spatial distribution of the mica phase within studied granites were obtained. Tomography data were compared to results provided by other experimental methods commonly used in rock mechanics research such as optical and electron microscopy, as well as ultrasonic shear-wave measurements. The benefits and limitations for application of the neutron tomography method for studies of granite like rocks are discussed.
The effect of sapphire and bismuth single-crystal filters and their combinations on the quality of neutron radiographic images and neutron tomography data has been studied. The parameters of the contrast of the neutron image were analyzed depending on the monocrystalline filters. Neutron transmission spectra were obtained for sapphire and bismuth single crystals. Additionally, the effect of filters on the overall intensity of the thermal neutron beam and the background of gamma-rays was investigated. Based on the obtained data, we assume that a single-crystal sapphire filter can be most effectively used for radiographic and tomographic installations using thermal neutrons.
The rock fabric of two lamprophyre dike samples from the Koy-Tash granitoid intrusion (Koy-Tash, Jizzakh region, Uzbekistan) has been studied, using the neutron tomography method. We have performed virtual segmentation of the reconstructed 3D model of the tabular igneous intrusion and the corresponding determination of dike margins orientation. Spatial distributions of inclusions in the dike volume, as well as further analysis of size distributions and shape orientations of inclusions, have been obtained. The observed shape preferred orientations of inclusions as evidence of the magma flow-related fabric. The obtained structural data have been discussed in the frame of the models of rigid particle motion and the straining of vesicles in a moving viscous fluid.
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