To accomplish rapidly the granulation process of digestion sludge for the treatment of actual coking wastewater and meanwhile achieve high COD, phenol, SCN- and CN- removal, the EGSB reactor was employed with two operation stages. StageI: Granular sludge was formed from digestion sludge using brewery wastewater as substrate in the anaerobic way (meanwhile adding little granules, which were 1/7 of the total biomass). StageII: Granular sludge was acclimatized with the actual coking wastewater through continuous micro-oxygenation way. The experimental results showed that the granular sludge could quickly form in 10d in the EGSB reactor seeded with digestion sludge and little loose granules. It took only about 6 months for the successful micro-aerobic acclimating of the granular sludge by the actual coking wastewater. The removal efficiencies of COD, phenol, SCN- and CN- were 72.9, 99.5, 95.7 and 97.5%, respectively, at 12.1h hydraulic retention time (HRT) and for 631-922, 12.8-37.7, 66.7-232.7 and 0.3-57.8mg.L-1 influent COD, phenol, SCN- and CN- concentration.
The effects of fuel quality and pollution control devices on SOF and PAHs emissions in particle matter (PM) for China V heavy-duty (HD) diesel engine fueled with China III, China IV and China V diesel were studied by using soxhlet extraction technique and Gas Chromatography-Mass Spectroscopy (GC-MS) technique. Two engines used were equipped with Diesel Oxidation Convert (DOC)+Diesel Particulate Filter (DPF) and Select Catalytic Reduction (SCR) individually. It is found that the SOF mass fraction in PM rises remarkably and total PAHs concentration declines obviously with the improvement of diesel fuel from China III to China V. However, the 16 components of PAHs distribute similarly for three quality of diesel, the concentrationes of Flu、PA、Ant、FL、Pyr、BaA、CHR reduce obviously, especially Pyr decrease by 95.8%. Moreover, the pollution control device has important effects on SOF and PAHs emissions.
Coupled anaerobicaerobic granular bio-film reactor was employed to acclimatize the granules when treating actual coking wastewater. Two oxygenation methods (i.e. A and B) were employed. For method A, dissolved O2 was supplied to the reactor A (RA) through a continuous oxygenation way of 800-15000mlmin-1. And for method B, dissolved O2 of 800-15000mlmin-1 (18-12 times at 20-60min intervals, 1 h each time) was supplied to the reactor B (RB). The experimental results showed that it took only about 6 months for granules acclimation using actual coking wastewater. With inorganic carbon (NaHCO3) addition, both oxygenation methods could run well when acclimatizing the granules. However, method A could have comparatively high and stable operation effect. And the continuous oxygenation way was more suitable for the acclimation of the granules when treating actual coking wastewater than the intermittent oxygenation way.
To determine the operation parameters of the expanded granular sludge bed (EGSB) reactor treating actual domestic wastewater at ambient temperature of 15-26°C, the effects of influent flow, HRT, recycle ratio,Vup and temperature on the performance of the EGSB reactor were investigated in this paper. The results indicated that when treating actual domestic wastewater, the EGSB reactor could support high influent flow and low HRT. For 9L.h-1, 11L.h-1, 15L.h-1, 24L.h-1 influent flow, with the optimal recycle ratios of 1.6-2.5, 1.2-1.6, 0.4-0.8, 0.0, the COD removal efficiencies could attain to 86-90%, 88-89%, 83%, 83%, respectively. For lower influent flow, higher Vup could slightly increase COD removal, but accordingly higher recycle ratio need to supply. Meanwhile, for higher influent flow, higher Vup will damage the granular characteristic and thus cause the decreasing of COD removal, and thus for the EGSB reactor treating actual domestic wastewater, 2.7-3.0m.h-1 optimal Vup should be employed. The EGSB reactor could work well at ambient temperature of 15°C-26°C. The optimal influent flow and Vup were 15-24L.h-1 and 3.0m.h-1. High average OLR of 18.6kgCOD.m-3.d-1 and high average COD removal efficiencies of above 81.4% could achieve, and only very low recycle ratio of 0.0 to 0.4 need employ.
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