-Laser beam cutting is one important nontraditional machining process. This paper optimizes the parameters of laser beam cutting parameters of stainless steel (316L) considering the effect of input parameters such as power, oxygen pressure, frequency and cutting speed. Statistical design of experiments is carried in three different levels and process responses such as average kerf taper (T a ), surface roughness (R a ) and heat affected zones are measured accordingly. A response surface model is developed as a function of the process parameters. Responses predicted by the models (as per Taguchi's L 27 OA) are employed to search for an optimal combination to achieve desired process yield. Response Surface Models (RSMs) are developed for mean responses, S/N ratio, and standard deviation of responses. Optimization models are formulated as single objective optimization problem subject to process constraints. Models are formulated based on Analysis of Variance (ANOVA) and optimized using Matlab developed environment. Optimum solutions are compared with Taguchi Methodology results. As such, practicing engineers have means to model, analyze and optimize nontraditional machining processes. Validation experiments are carried to verify the developed models with success.
Molybdenum carbide co-catalyst and carbon nanofiber matrix are suggested to improve the nickel activity toward methanol electrooxidation process. The proposed electrocatalyst has been synthesized by calcination electrospun nanofiber mats composed of molybdenum chloride, nickel acetate, and poly (vinyl alcohol) under vacuum at elevated temperatures. The fabricated catalyst has been characterized using XRD, SEM, and TEM analysis. The electrochemical measurements demonstrated that the fabricated composite acquired specific activity for methanol electrooxidation when molybdenum content and calcination temperature were tuned. In terms of the current density, the highest performance is attributed to the nanofibers obtained from electrospun solution having 5% molybdenum precursor compared to nickel acetate as a current density of 107 mA/cm2 was generated. The process operating parameters have been optimized and expressed mathematically using the Taguchi robust design method. Experimental design has been employed in investigating the key operating parameters of methanol electrooxidation reaction to obtain the highest oxidation current density peak. The main effective operating parameters of the methanol oxidation reaction are Mo content in the electrocatalyst, methanol concentration, and reaction temperature. Employing Taguchi’s robust design helped to capture the optimum conditions yielding the maximum current density. The calculations revealed that the optimum parameters are as follows: Mo content, 5 wt.%; methanol concentration, 2.65 M; and reaction temperature, 50 °C. A mathematical model has been statistically derived to describe the experimental data adequately with an R2 value of 0. 979. The optimization process indicated that the maximum current density can be identified statistically at 5% Mo, 2.0 M methanol concentration, and 45 °C operating temperature.
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