High-purity anatase TiO2nanoparticles were prepared using an improved sol-hydrothermal method. The as-prepared sample was characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), Brunauer-Emmett-Teller (BET), and UV-vis diffuse reflectance spectra. TEM results showed that the average particle size of all TiO2particles was calculated to be (10±1) nm. The XRD analysis indicated that the present sample was fully crystallized and appeared to be highly phase-pure anatase. The BET analysis showed that the as-prepared sample had a very large specific surface area of 186.25 m2/g. The photocatalytic performance of TiO2nanoparticles was evaluated by photocatalytic degradation of X-3B and X-BR solutions. The degradation results revealed that the as-prepared TiO2showed slightly higher photocatalytic activities than P25. Whereas, the as-synthesized TiO2can settle down and be separated easily after the photocatalytic reaction finishes.

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