Three simple and low-cost configurations of handheld scanning probes for optical coherence tomography have been developed. Their design and testing for dentistry applications are presented. The first two configurations were built exclusively from available off-the-shelf optomechanical components, which, to the best of our knowledge, are the first designs of this type. The third configuration includes these components in an optimized and ergonomic probe. All the designs are presented in detail to allow for their duplication in any laboratory with a minimum effort, for applications that range from educational to high-end clinical investigations. Requirements that have to be fulfilled to achieve configurations which are reliable, ergonomic—for clinical environments, and easy to build are presented. While a range of applications is possible for the prototypes developed, in this study the handheld probes are tested ex vivo with a spectral domain optical coherence tomography system built in-house, for dental constructs. A previous testing with a swept source optical coherence tomography system has also been performed both in vivo and ex vivo for ear, nose, and throat—in a medical environment. The applications use the capability of optical coherence tomography to achieve real-time, high-resolution, non-contact, and non-destructive interferometric investigations with micrometer resolutions and millimeter penetration depth inside the sample. In this study, testing the quality of the material of one of the most used types of dental prosthesis, metalo-ceramic is thus demonstrated.
Some forensic in situ investigations, such as those needed in transportation (for aviation, maritime, road, or rail accidents) or for parts working under harsh conditions (e.g., pipes or turbines) would benefit from a method/technique that distinguishes ductile from brittle fractures of metals-as material defects are one of the potential causes of incidents. Nowadays, the gold standard in material studies is represented by scanning electron microscopy (SEM). However, SEM instruments are large, expensive, time-consuming, and lab-based; hence, in situ measurements are impossible. To tackle these issues, we propose as an alternative, lower-cost, sufficiently high-resolution technique, Optical Coherence Tomography (OCT) to perform fracture analysis by obtaining the topography of metallic surfaces. Several metals have been considered in this study: low soft carbon steels, lamellar graphite cast iron, an antifriction alloy, high-quality rolled steel, stainless steel, and ductile cast iron. An in-house developed Swept Source (SS) OCT system, Master-Slave (MS) enhanced is used, and height profiles of the samples' surfaces were generated. Two configurations were used: one where the dimension of the voxel was 1000 µm 3 and a second one of 160 µm 3 -with a 10 µm and a 4 µm transversal resolution, respectively. These height profiles allowed for concluding that the carbon steel samples were subject to ductile fracture, while the cast iron and antifriction alloy samples were subjected to brittle fracture. The validation of OCT images has been made with SEM images obtained with a 4 nm resolution. Although the OCT images are of a much lower resolution than the SEM ones, we demonstrate that they are sufficiently good to obtain clear images of the grains of the metallic materials and thus to distinguish between ductile and brittle fractures-especially with the higher resolution MS/SS-OCT system. The investigation is finally extended to the most useful case of fatigue fracture of metals, and we demonstrate that OCT is able to replace SEM for such investigations as well.
We demonstrate the capability of optical coherence tomography (OCT) to perform topography of metallic surfaces after being subjected to ductile or brittle fracturing. Two steel samples, OL 37 and OL 52, and an antifriction Sn-Sb-Cu alloy were analyzed. Using an in-house-built swept source OCT system, height profiles were generated for the surfaces of the two samples. Based on such profiles, it can be concluded that the first two samples were subjected to ductile fracture, while the third one was subjected to brittle fracture. The OCT potential for assessing the surface state of materials after fracture was evaluated by comparing OCT images with images generated using an established method for such investigations, scanning electron microscopy (SEM). Analysis of cause of fracture is essential in response to damage of machinery parts during various accidents. Currently the analysis is performed using SEM, on samples removed from the metallic parts, while OCT would allow in situ imaging using mobile units. To the best of our knowledge, this is the first time that the OCT capability to replace SEM has been demonstrated. SEM is a more costly and time-consuming method to use in the investigation of surfaces of microstructures of metallic materials.
We present our experience regarding the establishing of an interdisciplinary group with Optics as one of its main topic at the Aurel Vlaicu University of Arad (UAVA) -linked with the improvement through research of our educational activities. The 3OM Group (in Opto-Mechatronics, Optical Metrology, and Optics & Mechanics) is described in its evolution from optomechanics to photonics, the latter with a focus on OCT (Optical Coherence Tomography) -with the national and the international collaborations established, with universities from Romania, Europe and USA. While the research directions of the 3OM Group are presented, they are linked with the educational components implemented in the various subjects we teach, for both undergraduate and graduate students, both in Mechanical and in Electrical Engineering. The main effort is to integrate education and research, to move teaching beyond the classical aspects to put the stress on hands-on-experiments, as well as on research-based activities -even with undergraduates. The main goals of this approach are to obtain an early orientation towards innovation and discovery, with a taste for novelties and with a clear focus on international standards. While this account is only one of many, it offers our experience in passing through the difficulties of developing both research and education in Optics in a young university in an emergent economy in Eastern Europe.
We present our efforts in establishing a Research Pole in Photonics in the future Arad-Timisoara metropolitan area projected to unite two major cities of Western Romania. Research objectives and related training activities of various institutions and groups that are involved are presented in their evolution during the last decade. The multi-disciplinary consortium consists principally of two universities, UAVA (Aurel Vlaicu University of Arad) and UMF (Victor Babes Medicine and Pharmacy University of Timisoara), but also of the Arad County Emergency University Hospital and several innovative SMEs, such as Bioclinica S.A. (the largest array of medical analysis labs in the region) and Inteliform S.R.L. (a competitive SME focused on mechatronics and mechanical engineering). A brief survey of the individual and joint projects of these institutions is presented, together with their teaching activities at graduate and undergraduate level. The research Pole collaborates in R&D, training and education in biomedical imaging with universities in USA and Europe. Collaborative activities, mainly on Optical Coherence Tomography (OCT) projects are presented in a multidisciplinary approach that includes optomechatronics, precision mechanics and optics, dentistry, medicine, and biology.
To determine the roughness is an important aspect in both industrial and biomedical applications. We propose and utilize for roughness evaluations, a non-destructive evaluation methods, Optical Coherence Tomography (OCT). For the metallic surfaces investigated from this point of view, the Ra and Rz parameters are utilized, according to ISO 4287/1988. Also, according to ISO 4280 and ISO 3274 standards, the measurements have been made on 12.5 mm portions. In order to accommodate such evaluations with the specific OCT field-of-view, four consecutive OCT images have been made for each sample, and an appropriate processing of the data collected from the surface profiles has been made. A validation of the results obtained with OCT has been completed with the gold standard for such evaluations, using a contact mechanical method, with a Mitutuyo profiler.
Metals can break either in a ductile or brittle manner if a static or dynamic load is applied to the same material. This depends on a variety of factors, such as the manner in which the load is applied, the shape of the mechanical part, the operating conditions, the nature and structure of the metallic material, and the working temperature. If subjected to variable loads, metallic materials break due to what is called fatigue. The microscopic analysis of fracture surfaces is currently carried out by using scanning electron microscopy (SEM). We have proposed, for the first time to our knowledge, a new method to analyze fracture surfaces, using a low coherence interferometry technique, Optical Coherence Tomography (OCT) [Gh. Hutiu, V.-F. Duma, et al., Surface imaging of metallic material fractures using optical coherence tomography, Appl. Opt. 53, 5912-5916 (2014); Gh. Hutiu, V.-F. Duma, et al., Assessment of ductile, brittle, and fatigue fractures of metals using optical coherence tomography, Metals 8, 117 (2018)]. The present paper presents the way we have demonstrated that OCT can replace the gold standard in such assessments, i.e. SEM, despite the fact that OCT has a resolution of 20 to 4 μm (in our investigations), while the SEM we employed has a 4 to 2 nm resolution. A few examples are given in this respect-for different types of fractures. The advantages of OCT versus SEM are discussed. This development opens the way for in situ investigations, for example in forensic sciences, where OCT can be applied (including with handheld scanning probes. as we have developed). In contrast, SEM, TEM, and AFM are lab-based techniques, more expensive, and they require trained operators.
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