REACTION OF R~ETHANESULFINYL CHLORIDE WITH WATER
3645and lithium aluminum hydride in T H F was refluxed for 20 min before work-up to afford 0.83 g (28%) of phenylacetonitrile and 0.83 g (25%) of recovered phenylacetamide. As before, the B. With Benzamide.--To a solution of 3.025 g (0.025 mole) ered, mp, mmp 127-129'. another experiment on four times the scale.A similar result was obtained in remainder of the product consisted of tarry materials.
Bei der Hydrolyse des Peptids (Ia) entstehen neben der freien Säure (Ib) über eine Es‐Eliminierung das Dehydro‐alanin‐peptid (II) sowie das Disulfid (III).
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