A comparison between thermal poling of silica in air and in vacuum is reported. It is shown that the second-order susceptibility and thickness of the nonlinear layer as well as their time evolution are highly dependent on the surrounding poling atmosphere. In the vacuum case a charge distribution (under the anode) more complex and broader than that for the air case has also been revealed by laser induced pressure pulse measurements. A multiple charge carrier model can explain the formation and evolution of the depletion region under the anode. The findings are relevant to achieve improved nonlinearities in fiber and waveguide devices.
We fabricated second-order nonlinear gratings in D-shaped germanosilicate fibers, using thermal poling and periodic electrodes defined by standard photolithography. These gratings, which are up to 75 mm long, were used for efficient quasi-phase-matched frequency doubling of 1.532-mum nanosecond pulses from a high-power erbium-doped fiber amplifier. Average second-harmonic powers as high as 6.8 mW and peak powers greater than 1.2 kW at 766 nm were generated, with average and peak conversion efficiencies as high as 21% and 30%, respectively.
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