Aging of motor oil is characterized
by diverse NMR methods to get insight into the chemical processes
which occur during aging. Already one-dimensional 1H and 13C spectra reveal the relevance of chemical aging also with
respect to the mechanical behavior of oils. As NMR is a quantitative
analytical method, the absolute chemical changes can be observed and
quantified. In addition, the spectral interpretation in terms of chemical
composition is confirmed and deepened by two-dimensional 1H–1H, 1H–13C, and 1H–15N correlation spectra, as well as diffusion
and relaxation experiments. The different NMR results are discussed
and interpreted to obtain a thorough picture about aging processes
of motor oils.
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