Aims:To evaluate the effect of storage pH on solubility of white mineral trioxide aggregate (WMTA), bioaggregate (BA), and nano WMTA cements.Materials and Methods:Forty-eight moulds randomly allocated into three groups of pH 4.4 (group A), 7.4 (group B), and 10.4 (group C); and one empty as control in each group. Each group was further divided into three subgroups according to the material studied; WMTA, BA, and nano WMTA. The specimens in subgroup A were soaked in butyric acid buffered with synthetic tissue fluid (STF) (pH 4.4), while the samples in subgroups B (pH 7.4) and C (pH 10.4) buffered in potassium hydroxide for 24 h and then the loss of cement was determined. A two-way analysis of variance (ANOVA) and Tukey post-hoc statistical tests were used to detect any statistically significant differences among the groups/subgroups.Results:Statistical analysis has showed the highest solubility in acidic pH for all tested materials. Nano WMTA samples in pH = 10.4 had the lowest and BA samples in pH = 4.4 showed the highest cement loss.Conclusion:The solubility of all tested cements can be jeopardized in acidic environment which might affect on their sealing characteristic in clinical scenario. However, nano WMTA cement due to its small size particles and different additives was capable of producing lower porosity in set material, which resulted in showing more resistance in acidic environment.
Introduction: The thickness threshold for detecting endodontic biomaterials depends on many factors, such as the nature of the radiopacifier and the particle size. Aim: The aim of this study was to determine the effect of thickness on radiodensity of various endodontic biomaterials; and evaluate the impact of radiopacifier particle size on radiodensity. Materials and Methods: This in-vitro study was conducted between August 2018 to December 2019. The study was divided in two parts, in first part, Six endodontic biomaterials (AH26, EndoSequence, Endoseal Mineral Trioxide Aggregate (MTA), Nano-MTA, Endocem Zr, and MTA without radiopacifier) were selected and evaluated in different thicknesses, in second part, MTA mixed with Bismuth oxide 10 μm, 200 μm, 120 nm (Groups 1-3), and Zirconium oxide 5 μm, 1 μm and 20 nm (Groups 4-6) were placed in frames with 1 mm, 0.5 mm, 0.2 mm, 0.1 mm thicknesses to evaluate the radiopacity. Results: The mean radiodensity was significantly different among various thickness (p<0.001) and materials (p<0.001). The changes of the radiodensity in various thickness from one material to the other were not uniform (interaction p-value <0.001). A 1 mm thickness had highest radiodensity (206.6±83.99), followed by 0.5 mm (68.9±24.6), 0.2 mm (17.9±4.9), and 0.1 mm thick material had least radiodensity (11.97±4.37). Materials of AH26 (99.1±103.2), Nano MTA (97.4±104.9), Endoseal MTA (87.86±101.4), Endosequence BC sealer (85.5±93.87) and Endocem Zr (71.88±77.67) were significantly different from the control group (16.38±10.85). The size of particles played important role in radiodensity (p<0.001). The radiodensity of Fine GIII (100 nm) material (112.68±108.47) was significantly higher than other materials: Thin GII (200 nm) (100.9±102.4), Fine GVI (20-40 nm) (99.7±95.1), Coarse GI (10 μm) (76.66±74.75), Thin GV (1~3 μm) (63.19±67.3), Coarse GIV (5 μm) (49.66±51.59) and MTA without Radiopaque Agent GVII (100%) (23.67±19.68). The effect of the thickness on radiodensity was different for each biomaterial, with significant differences from the control group. Conclusion: One of the readily available methods for increasing radiodensity is to increase the amount of radiopacifier, which might compromise the physical properties of the material. Fine particle radiopacifier (120 nm) with 1 mm thickness has significantly higher radiodensity than any other biomaterials in this study. Within the limitations of the current study, it can be concluded that the radiopacifier particle size has a significant impact on the level of radiodensity of dental biomaterials. Finding the optimum distribution, size, and geometry of radiopacifier particles within the same fraction rate can enhance the radiodensity.
Objective:To evaluate the effects of deionised water, blood, phosphate-buffered saline (PBS) and a new anti-corrosive solution based on methoxy propyl amine (MOPA) on the cyclic fatigue resistance of endodontic NiTi rotary instruments under in vitro conditions. Methods: Forty ProTaper F1 files were provided and divided to four groups (n=10). Samples were first autoclaved and then stored in deionised water, blood, PBS or MOPA for 24 hours. Cyclic fatigue was tested with a custom-made stainless-steel block including artificial canals (curvature angle=30 degree, radius of curvature=5 mm). After immersion in test solutions, samples were rotated 300 rpm until fracture occurred. The number of cycles to failure (NCF) was calculated using recorded fracture time. Results: Data were analysed by the Kolmogorov-Smirnov, Levene, ANOVA and Scheffe statistical tests. Samples in blood group showed the lowest and samples in MOPA group showed the highest NCF values. Significant difference was observed between groups (p=0.001). NCF value of PBS group was significantly more than the NCF values of samples in blood and deionised water groups (p<0.05). Conclusion:The tested novel anti-corrosive solution significantly increased the fracture resistance of the endodontic NiTi rotary instruments by reducing the cyclic fatigue. In contrast, blood and deionised water caused more corrosion and resulted in earlier file fracture. Keywords: anti-corrosion, cyclic fatigue, NCF, NiTi rotary INTRODUCTIONThe advent of NiTi rotary instruments to the field of endodontic was a revolutionary change. These devices are made of pseudo-elastic alloy of nickel and titanium (Nitinol 55) and have an incredible influence on the mechanical preparations of root canals (1). The instrumentation of narrow and curved root canals can be challenging for many clinicians. Walia et al. showed that Nitinol files are at least two to three times more flexible than stainless steel (SS) files (2). The flexibility can enable the instrument to be used in curved and complex root canals with more facility and lower root canal shape alterations (3).Many investigators have shown that the unexpected separation of NiTi rotary instruments, apart from higher strength and flexibility, remains a clinical challenge. This undesirable event can occur without any significant deformation seen on the surface of instrument (4). Different causes, such as cyclic fatigue, static and dynamic torsional fatigues, have been attributed to the fracture of these devices (5). Cyclic fatigue is described by the alternating tension and compression cycles, which occur inside the structure of an instrument when it is moving through the maximum curvature of root canal (6). The cyclic fatigue is generally a concern in curved canals, and the many ABSTRACT HIGHLIGHTS• Deionized water and blood can negatively influence the structure of NiTi made devices. • Methoxy propyl amine (MOPA) novel solution is an anti-corrosive agent, which can increase the cyclic fatigue resistance and delay separation of NiTi made rotary...
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