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This study was conducted to assess the representativeness of laboratory sampling protocols for purposes of trace metal analysis in soil. Five laboratory protocols were compared, including conventional grab sampling, to assess the influence of sectorial splitting, sieving, and grinding on measured trace metal concentrations and their variability. It was concluded that grinding was the most important factor in controlling the variability of trace metal concentrations. Grinding increased the reproducibility of sample mass reduction by rotary sectorial splitting by up to two orders of magnitude. Combined with rotary sectorial splitting, grinding increased the reproducibility of trace metal concentrations by almost three orders of magnitude compared to grab sampling. Moreover, results showed that if grinding is used as part of a mass reduction protocol by sectorial splitting, the effect of sieving on reproducibility became insignificant. Gy's sampling theory and practice was also used to analyze the aforementioned sampling protocols. While the theoretical relative variances calculated for each sampling protocol qualitatively agreed with the experimental variances, their quantitative agreement was very poor. It was assumed that the parameters used in the calculation of theoretical sampling variances may not correctly estimate the constitutional heterogeneity of soils or soil-like materials. Finally, the results have highlighted the pitfalls of grab sampling, namely, the fact that it does not exert control over incorrect sampling errors and that it is strongly affected by distribution heterogeneity.

This paper presents the results of Swedish fall cone tests and Casagrande liquid limit tests conducted on saline Champlain Sea clay samples from Lachenaie, Quebec. The main objective was to study a few hitherto unanswered practical questions regarding these testing methods. Penetration range is found to affect the Hansbo's relationship used in fall cone experiments, while the mass and the bluntness degree of the cone have no effect on it. A direct relationship between thixotropic regain in shear strength and sensitivity is found. When measuring the liquid limit, if only the first penetration depth is recorded, results are up to 5% smaller than those obtained when following the standard procedure of CAN/BNQ-2501-092.With this standard, the average of the first two penetration depths within 0.3 mm of each other is recorded. These penetrations usually follow the bulk of the thixotropic shear strength regain.The Swedish fall cone was compared to the traditional Casagrande apparatus for liquid limit determinations. The two methods yielded identical results in the studied conditions (saline Lachenaie clay with liquid limit between 44% and 75%). An incorrect calibration of the height-of-drop of 1.4 mm led to a mean error of 6 liquid limit points. This error is greater than the theoretical error obtained by assuming that the number of blows is proportional to the square of the height-of-drop.

SUMMARYThis paper presents a new interpretation method for pulse tests, a field permeability test that allows for rapid measurements of hydraulic conductivity k in aquitards. This new method applies to soft clay deposits. To initiate a pulse test, a known volume of water is injected into the sand filter of a monitoring well isolated by a packer. The resulting pressure increase yields an outward movement of the sand filter cavity wall. After presenting the usual interpretation methods and their limits, this paper proposes a new interpretation method based on a coupled analysis of the pressure and displacement fields in the soil using the Biot–Darcy formulation. A series of analytical and numerical non‐dimensional velocity graphs, normalized plots of the mean hydraulic head difference versus its rate of change, are given. For a linear elastic material, these type curves show relatively small variations with the sand filter aspect ratio and the Poisson ratio of the tested clay. The type curves are also found to be independent of the clay compressibility (mv) and k, an important result. A series of pulse tests conducted in a soft marine clay deposit near Montreal, Canada, are interpreted with the proposed method. The hydraulic conductivity values calculated from these tests are closely correlated with independent estimates obtained using long‐duration variable‐head tests. Compared with previous interpretation methods, the proposed method allows soil volume changes to be reconciled with cavity expansion phenomena and the range of type curves available for the interpretation of test data to be constrained. Copyright © 2013 John Wiley & Sons, Ltd.