Metathesis of propene to ethene and 2-butenes was studied over a series of MoO x /SBA-15 catalysts (molybdenum oxide supported on mesoporous silica SBA-15; Mo loading 2.1~13.3 wt%, apparent Mo surface density 0.2~2.5 nm -2
The fluorine content of polymer particles labelled with 2,2,2-trifluoroethylamine was reliably quantified with overlapping sensitivity ranges by XPS and solid-state NMR. This provides a first step towards reference materials for the metrological traceability of surface group quantifications. The extension of this concept to fluorescence spectroscopy is illustrated.
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