In this study, the mechanical and fracture behaviour of marine sandwich-structured composite that is manufactured by vacuum-assisted resin infusion process with a PVC foam-web core, and different thicknesses of upper and lower glass fibre-reinforced polymer face sheets used as outer and inner side of the hull have been examined. The properties of PVC core, face sheet material, and composite sandwich structures are presented. Failure modes include sandwich flatwise tension, core flatwise compression, sandwich edgewise compression, and face sheet bending of manufactured composites have been investigated experimentally for marine application. The analytical solution is derived to calculate the flexural rigidity, shear stresses and maximum tensile, compression stresses in three-point bending specimens for marine sandwich composites. 3 End Notched Flexure test method has been applied to calculate the strain energy release rate. Moreover, the finite element study is carried out by using a 2D model to calculate the fracture energy (J) value numerically and virtual crack closure technique. Reasonably good results are obtained between analytical and numerical methods.
High entropy alloys (HEA) are one of the modern-era alloys accelerating with greater velocity because of their excellent properties and different applications. In the present paper, we have successfully fabricated HEA (23Fe-21Cr-18Ni-20Ti-18Mn) powders by ball milling the elemental Fe, Cr, Ni, Ti, and Mn powders for 15 h. The advancement of the milling process and phase transformation of HEAs were studied by using X-ray diffraction (XRD) and scanning electron microscope (SEM). The crystallite size and the lattice strain of the HEA were calculated by using the Williamson-Hall (W-H) equation and the values were found to be 7 nm and 0.0176%, respectively. Similarly, the true lattice parameter was calculated using the Nelson–Riley (N-R) extrapolation method, and the value was found to be 3.544 Å. We have successfully investigated the electrochemical response of 15 h ball milled 23Fe-21Cr-18Ni-20Ti-18Mn HEA powders to determine the ascorbic acid (AA) using cyclic voltammetry. We have modified the carbon paste electrode with ball milled HEA of concentrations 0, 2, 4, 6, 8, and 10 mg, and among them, 8 mg HEA modified carbon paste electrode (HEA-MCPE) depicted the highest current sensitivity. We reported the effect of modifier concentration, analyte concentration, scan rate, and pH on the oxidation peak of AA. The electrochemical active surface area of carbon paste and MCPE was calculated using the Nernst equation and the values were found to be 0.0014 cm2 and 0.0027 cm2, respectively. The fabricated HEA-MCPE showed excellent current sensitivity, stability, anti-fouling, and selectivity.
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