This paper presents the design, construction, and assembly of laboratory apparatus to undertake in‐situ corrosion fatigue tests in a sour corrosive environment under uniaxial fatigue loading. The bespoke test cell allows periodic nondestructive X‐ray micro‐computed tomography of the specimen in‐situ during fatigue testing and thus enables monitoring of material degradation in‐situ as it progresses and in particular the pit‐to‐crack transition. This approach provides more direct information on crack initiation than complementary ex‐situ techniques such as scanning electron microscopy of post‐test metallographic specimens. Moreover, the apparatus was designed to allow a fatigue cycle to be interrupted and maintain the sample under static tensile load, during X‐ray tomography scans. This process reduced the risk of premature crack closure during interrupted tests. Results presented herein demonstrate the performance and reliability of our approach and will hopefully stimulate other groups to use similar “lab‐scale” initiatives.
The environmental performance of 316L grade stainless steel, in the form of tensile specimens containing a single corrosion pit with various aspect ratios, under cyclic loading in aerated chloride solutions is investigated in this study. Results from environmental tests were compared and contrasted with those obtained using finite element analysis (FEA). Fractography of the failed specimens obtained from experiments revealed that fatigue crack initiation took place at the base of the shallow pit. The crack initiation shifted towards the shoulder and the mouth of the pit for pits of increasing depth. This process is well predicted by FEA, as the strain contour maps show that strain is the highest around the centric strip of the pit. However, for shallow pits, local strain is uniformly distributed around that strip but begins to concentrate more towards the shoulder and the mouth region for increasingly deep pits.
Corrosion pits are a form of geometrical discontinuity that lead to stress and strain concentration in engineering components, resulting in crack initiation under service loading conditions and ultimately fracture and failure. Initiation and propagation of cracks in offshore pipelines can lead to loss of containment and environmental and commercial impacts. In order to prevent such failures, tools to predict the structural integrity of pipelines need to be improved. This work investigates the fatigue behaviour of corrosion pits in API-5L X65 grade steel pipeline utilising numerical and analytical methods. Firstly, load-controlled fatigue tests were carried out on smooth X65 steel samples to establish S–N data. Secondly, local stress–strain behaviour at corrosion pits and its effect on fatigue crack initiation were investigated using elastic-plastic finite element analysis of samples containing a single corrosion pit under cyclic loading. Analysis of stabilised stress–strain hysteresis loops at corrosion pits showed that the local stress ratio at the pit changes from 0.1 to −0.4 while the applied stress amplitude increases with the same stress ratio of 0.1. Analytical methods were also used to predict the local maximum stress and strain at the pit, which showed a similar local stress ratio to the finite element analysis result but lower stress and strain ranges. Finally, fatigue crack initiation life was predicted using the combination of finite element stress and strain analysis and the Smith–Watson–Topper strain–life approach. An advantage of this method for life estimation is that this approach considers the local stress and strains at corrosion pits rather than applied stress.
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