Abstract.[Hg(C2H302)(C6H5S)] , M r --368"80, monoclinic, P2Jn, a=18.362(2), b=7.485(1), c= 14.292 (2)/~, fl= 104.72 (1) °, V= 1900.0 (3) ,/k 3, Z = 8, D x = 2.58 g cm -3, 2(Mo Ka) = 0.71069 ,/k, /t = 164 cm -~, F(000) = 1344, T= 295 K, R = 0.034 for 2326 unique observed reflections. The structure is built up of infinite -S-Hg-Schains linked via acetate groups into sheets. The two independent Hg atoms, five-and six-coordinated, are in addition to the two thiolate groups also bonded to two and three acetate ligands, respectively.
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