Aim:The aim of this study was to evaluate the microhardness of two composite resins when subjected to three different temperatures and three different light-curing times.Materials and Methods:Two composites were used; Filtek Z250 and Grandio. Three different temperatures (23, 37, and 55oC) were used, utilizing a composite warmer. The heated samples were immediately injected into cylindrical molds (6 mm × 2 mm) and the top surface of the specimens was polymerized for 10, 20, and 40 sec, using a Quartz-Tungsten-Halogen light-curing unit (QTH LCU). Vickers microhardness measurements were performed from both the top and bottom surface of the specimens, following dry storage for 24 hours in the dark. Statistical analysis were performed using one-way analysis of variance (ANOVA) and Tukey post-hoc test at a level of significance of a = 0.05.Results:The results indicated that there was an increase in microhardness as the temperature of the composite was increased for either the top or the bottom surface (P < 0.05). Furthermore, there was a general increase in microhardness for both composites as curing time increased (P < 0.05). The type of composites did not influence the surface microhardness (P > 0.05).Conclusions:Temperature of composites affects their surface microhardness. Also, light-curing time influence microhardness values of the composites tested.
Introduction:The purpose of this study was to examine the effect of different extraction media, including culture media, as well as storage times on the elution of monomers from modern dental composites.Materials and Methods:Four contemporary composite materials were tested: (a) Clearfil Majesty Esthetic (Kuraray), (b) Esthet X (DENTSPLY), (c) Filtek Silorane (3M ESPE), and (d) Admira (Voco). Forty-eight specimens were made. The specimens were stored in 1 ml of (a) artificial saliva, (b) Dulbecco's Modified Eagle Medium (DMEM), (c) DMEM plus 10% fetal bovine serum (FBS), and (d) ethanol 75%. The specimens were analyzed after 24 hours and after 1 week of storage. HPLC Liquid Chromatography was performed to analyze the extracted solutions. The statistical package SPSS 18 was used for the statistical analysis of the results.Results:All the materials tested released monomers that were consistent with the base composition of their resin matrix. Bisphenol-A (BPA) was detected in Clearfil Esthetic and EsthetX when ethanol 75% was used for storage. TEGDMA was released at a faster rate compared to the other monomers with most of the monomer eluted in the first 24 hours. The effect of storage solution and storage time on the elution of the same monomers varied between materials.Conclusions:There was a significant effect of time, storage solution, and material on the elution of the detectable unbound monomers. Unbound monomers were detected in culture media, which may lead to false-negative results in cytotoxicity tests of resin composite materials. BPA was detected in two of the tested materials.
The new antibacterial adhesive system maintained pulp vitality and primary odontoblastic function in infected nonexposed and exposed cavities but interfered with reparative dentine formation in infected pulpal exposures.
The purpose of this study was to investigate microleakage in V class composite restorations with total etch versus self-etching adhesives. Experiments were conducted in vivo and were also evaluated interfacial micromorphology. Forty class V cavities were prepared on the buccal surfaces of teeth in three healthy dogs. The cavities were randomly assigned into five groups of eight teeth and restored with one of the following adhesive systems: Etch and Prime 3.0/Definite flow/Definite, Prompt L-pop/Filtek flow/P-60, Admira bond/Admira Flow /Admira, Bond 1/Flow it/Alert, Stae/Wave/Glacier. After 60 days the animals were killed and the teeth were extracted. The teeth were then immersed in a solution of 0.5% basic fuchsin dye for 24 h, sectioned and scored for microleakage. Features of the tooth/restoration interfaces were also examined using Scanning electron microscopy. Student-Newman-Keuls and one-way anova revealed significance differences among the groups for overall wall scores (P < 0.05). The total-etch adhesives revealed significantly less microleakage scores than the self-etching adhesive systems tested. Wilcoxon Signed Ranks Test revealed significant differences between the occlusal and gingival microleakage scores for each adhesive restorative system, with the exception of Admira (P < 0.05).
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