An investigation has been carried out of the effects of tool probe shape and size on the formation of surface composite by uniformly distributing SiC particles into a surface layer of an A1050-H24 aluminium plate through friction stir processing (FSP). Tool probes of three different diameters (3, 5 and 7 mm) and four different shapes (circular with threads, circular without threads, square and triangular) have been used to fabricate the surface layers at rotation speeds of 1500-2250 rev min 21 and a travelling speed of 1?66 mm s 21 . The SiC particles were packed into a groove of 3 mm width and 1?5 mm depth cut on the aluminium plate and covered by an aluminium sheet of 2 mm thickness. A rotating tool was plunged into the plate through the cover sheet so that the tip of the probe reached beyond the bottom of the groove. As a result, it was found that the square probe dispersed the SiC particles homogeneously in the nugget zone compared with other probe shapes regardless of the rotation speeds. Furthermore, the distributed particles and also the aluminium matrix grain size became finer by the use of square probe than those of the other shapes. On the other hand, the wear rates of the square and triangular probes were higher than that of circular shape. The worn iron debris from the tool reacted with aluminium matrix and form fine iron aluminides compound dispersed in the nugget zone. The probe size had limited effects on the homogeneity of the SiC particles distribution in the nugget zone; the distribution of SiC particles obtained by triple FSP passes was less homogeneous when the probe size was smaller. Microhardness of the nugget zone was homogeneously increased to a level as high as 60 HV with tool of square probe shape after three passes to be compared with 23 HV of the aluminium matrix beside the nugget zone.
A feasibility investigation has been carried out of the formation of surface composite by uniformly distributing SiC particles 1?25 mm in size into a surface layer of an A 1050-H24 Al plate through friction stir processing (FSP). The SiC particle was filled into a groove cut on the Al plate, covered by an Al sheet 2 mm thick, and a rotating tool was penetrated from the cover sheet so that the probe tip reached a depth beyond the groove bottom. The effects of process parameters (rotation speed and travelling speed) and applying multiple passes on the distribution of SiC particle in the nugget zone were investigated. The effects of groove size and its position relative to the tool probe were also investigated. Applying multiple passes had a great effect on the homogeneity of the SiC particle distribution. At rotation speeds of 2000-3000 rev min 21 , the SiC particles tended to cluster in some places in the nugget zone. By decreasing the rotation speed to 1000-1500 rev min 21 , the SiC particle was distributed in almost all the nugget zone area when the groove was 2-3 mm wide and 1?5 mm deep. On the other hand, the stirring action of FSP was insufficient to distribute homogenously the SiC particles when the groove size was increased to 362 mm. By shifting the groove position towards the advancing side of the tool probe, the distribution of the SiC particles in the nugget zone became better. The defect free nugget zone with homogenously distributed SiC particles was obtained in a sample produced by FSP at rotation speeds of 1500 rev min 21 for the first pass and 1250 rev min 21 for the second and third passes. Microhardness of the nugget zone was increased to a level as high as 55 HV when the groove size was 361?5 mm. The effect of the rotation speed on the particles dispersion was discussed with particular reference to the vertical material flow in the nugget zone.
In the present work, in-situ metal matrix composites were fabricated through squeeze casting. The copper particles were dispersed with different weight percentages (3%, 6%, 10%, and 15%) into Al-12% Si piston alloy. Also, heat treatments were performed at 380 °C and 450 °C for holding times of 6 and 18 h. The microstructures, X-ray diffractometer (XRD) pattern, hardness, and wear characteristics were evaluated. The results showed that these copper particles have reacted with the aluminum under all of the aforementioned processing conditions resulting in the formation of fine copper aluminide intermetallics. Most of the intermetallics were CuAl2, while AlCu appeared in a small ratio. Additionally, these intermetallics were homogenously distributed within the alloy matrix with up to 6% Cu addition. The amounts of those intermetallics increased after performing heat treatment. Most of these intermetallics were CuAl2 at 380 °C, while the Cu-rich intermetallics appeared at 450 °C. Increasing the holding time to 18 h, however, led to grain coarsening and resulted in the formation of some cracks. The hardness of the resulting composite materials was improved. The hardness value reached to about 170 HV after heat treating at 380 °C for 8 h. The wear resistance of the resulting composite materials was remarkably improved, especially at lower additions of Cu and at the lower heat treatment temperature.
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