The fourteen membered biogenic tetraazamacrocycles and their complexes have taken a considerable position for their wide variety of applications. They are applicable in magnetic resonance imaging (MRI), pharmacological, radioimmunotherapy, analytical and industrial field. They are also well recognized due to their resemblance to the naturally occurring macrocyclic complexes. Keeping this in mind, here we are presenting a report on the characterization and antimicrobial activities of tetraazamacrocyclic ligands and their Palladium(II) and palladium(IV) complexes. The reactions of 3,
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