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Urea derivatives Q 0640 4-Acylamino-and 4-Ureidobenzamides as Melanin-Concentrating Hormone (MCH) Receptor 1 Antagonists -[synthesis, in vitro biological evaluation, and structure-activity relationships]. -(RECEVEUR, J.-M.; BJURLING, E.; ULVEN, T.; LITTLE, P. B.; NOERREGAARD, P. K.; HOEGBERG*, T.; Bioorg. Med. Chem. Lett. 14 (2004) 20, 5075-5080; 7TM Pharma A/S, DK-2970 Hoersholm, Den.; Eng.) -M. Schroeter 03-102

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Indol-1-yl-substituted dihydropyranyl- and cyclohexenylmolybdenum complexes were obtained via nucleophilic addition of a variety of substituted indoles to cationic (pyran)- and (cyclohexadiene)molybdenum complexes. The efficiency of these addition reactions was found to be highly dependent upon the substitution pattern in the nucleophile. Oxidative decomplexation with iodine smoothly delivered the corresponding allylic iodide in good yield. Complex 6b was characterized by X-ray crystallography.