In this paper, we report on a homemade optical spectrometer using diffraction grating and image processing techniques. This device was designed to produce spectral images that could then be processed by measuring signal strength (pixel intensity) to obtain the light source, transmittance, and absorbance spectra of the liquid sample. The homemade optical spectrometer consisted of: (i) a white LED as a light source, (ii) a cuvette or sample holder, (iii) a slit, (iv) a diffraction grating, and (v) a CMOS camera (webcam). In this study, various concentrations of a carbon nanoparticle (CNP) colloid were used in the particle size sample test. Additionally, a commercial optical spectrometer and tunneling electron microscope (TEM) were used to characterize the optical properties and morphology of the CNPs, respectively. The data obtained using the homemade optical spectrometer, commercial optical spectrometer, and TEM showed similar results and trends. Lastly, the calculation and measurement of CNP size were performed using the effective mass approximation (EMA) and TEM. These data showed that the average nanoparticle sizes were approximately 2.4 nm and 2.5 ± 0.3 nm, respectively. This research provides new insights into the development of a portable, simple, and low-cost optical spectrometer that can be used in nanomaterial characterization for physics undergraduate instruction.
Zero-dimensional Perovskite Magic-size Clusters play crucial roles in understanding and controlling nucleation and growth of semiconductor nanoparticles. However, their metastability behavior is a critical hindrance for reliable characterizations. Here, we report the first demonstration of using an excess amount of surface ligand and SiO2 as novel passivation for synthesizing the magic-sized clusters (MSCs) by the Ligand-assisted reprecipitation method. A synergetic effect between an excessed surface ligand and SiO2 inhibits the protonation and deprotonation reaction between amine-based and acid-based ligand, leading to enhanced PL stability. The obtained CH3NH3PbBr3 PMSCs/SiO2 retain 70% of its initial emission intensity in ambient conditions for 20 days. This passivation approach opens an entirely new avenue for the reliable characterizations of CH3NH3PbBr3 PMSCs, which will significantly broaden their application for understanding and controlling nucleation and growth of semiconductor nanoparticles.
Carbon nanoparticles (C-Dots) were synthesized using citric acid and urea as carbon and fuel source, and combustion reaction methods. The absorption spectral and morphology particles of C-Dots were investigated. The morphology describes the synthesis of small (<1 ?m) and monodispersedC-Dots. Thus, the C-Dots solutions has absorption spectral range of about 86% at visible light spectral. This study suggests that the as-prepared carbon nanoparticles (C-Dots) with particle size and absorption spectral tunability might be utilized as solar energy absorber material.Karbon nanopartikel (C-Dots) disintesis menggunakan asam sitrat dan urea sebagai sumber karbon dan bahan bakar, melalui reaksi pembakaran sederhana. Spektrum absorpsi dan morfologi partikel C-Dots diinvestigasi menggunakan UV-Vis Spectrometry dan analisis SEM. Hasil SEM menunjukan bahwa morfologi partikel C-Dots sangat kecil (<1 ?m) dan seragam. Selain itu, larutan C-Dots memiliki spektrum absopsi pada rentang sekitar 86% pada daerah cahaya tampak. Hasil studi ini menunjukan bahwa karbon nanopartikel (C-Dots) dengan ukuran partikel dan spektrum absorpsi yang dapat diatur, sehingga dapat digunakan sebagai material penyerap sinar matahari.
Free fall motion in air medium is only influenced by gravitation acceleration. However, there are several variables that caused the observations to be different with the concept. Variables, such as air drag and terminal velocity, are often teachers not presented in detail, causing misconceptions. This study aims to develop a simple experiment on free fall motion by identifying air drag and terminal velocity. The data in this study is the video of free fall motion of paper and scraper analyzed using Tracker video analyze. From the video analyzed, information is obtained in the form of time (t), track (l, θ), and velocity (v) of the object. This study shows that the air drag force increase unto the terminal velocity. The calculation of the drag coefficient giving the number of the paper 2,16 and the scraper 2,10. According to data analyzed, the air drag force is affected by the mass (m), area (A), and the air drag force (F<sub>D</sub>) with the linear correlation until it reaches the terminal velocity. The result of this study may use as references of free fall motion experiment with other objects and analyze.
This paper presents drag force analysis of free falling object using software tracker. We use video cupclips that have been embedded in this software. The video featured cupcakes to which hung a number of different paper clips were dropped simultaneously. We track the trajectory of free falling cupclips using the software to get the information of position, speed, and acceleration of each cupcake against time. From the data we get the value of drag forces and drag coefficients for each time. The result shows that the drag force value increased to almost constant value, otherwise the drag coefficient is reduced to almost constant values well. According to the results, the analyzed data has good agreement with the theory. Thus, software tracker can be used as media to learn drag force easily and inexpensively.
Abstract.Copper nanowires (CuNWs) for different synthesis temperatures were prepared by solution-grown method. The surface morphology and electrical resistance of CuNWs were investigated. The surface morphology analysis describes the synthesis of long (> 20μm), thin (< 60 nm), and mono-dispersed CuNWs. Thus, in the case of temperature treatment from 4 °C to 80 °C in water based solution, the CuNWs has diameter of about 71 nm, length up to 37 μm and electrical resistance (R) at 0.1 Ω. This study suggests that the as-prepared copper nanowires (CuNWs) with diameter and electrical resistance tunability might be utilized as flexible transparent conducting electrode.
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