The main purpose of the presented article is the preparation of novel glass-ceramics in CaO-SiO 2 -P 2 O 5 -MgO system and evaluation of carbonate apatite formation after soaking in TRIS-HCl buffer solution for 14 days. The investigated samples were prepared via sol-gel method and structure of the obtained samples was studied using XRD, FTIR, SEM, XPS and ICP-AES. XRD of the thermally treated samples showed that the presence of some crystalline phases is depended on the gel composition. FTIR revealed the existence of all characteristic bands for the observed crystalline phases. SEM monitored the presence of particles with different morphology. After soaking in TRIS-HCl solution, FTIR confirmed that carbonate apatite was formed on the soaked surface. The obtained data are in a good agreement with XPS analysis. The change of ions concentrations in TRIS-HCl buffer solution after immersion of the prepared glass-ceramics was recorded by ICP-AES measurements.
Wear resistance is an important rubber compound property related to useful product life. The rubber compound properties that affect wear behavior are very complicated. Wear is related to a rubber compound’s cut resistance, tear resistance, fatigue resistance hardness, etc. The most commonly used test method to determine the wear resistance of rubber materials is abrasion test. Tested compounds are usually compared on a “volume loss” basis which is calculated from the weight loss and density of the compound. This method is known to be variable and doesn’t give additional information for the wear behavior. For this reason we propose alternative approaches for examination of the wear behavior of rubber composites, giving information not only for the wear resistance but also for elastic the modulus, stiffness of the material, damage mechanism, etc. Continuous multi-cycle indentation is used to determine the indentation hardness, elastic modulus and the stiffness with two indenter types –Vickers and sphero-conical. Comparison of both results is made in order to investigate the effect of the indenter type.
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