The extractives of oil-tea cake are considered to have bioactive components, but the extracted residues of oil-tea cake are still not utilized. The analytical result by 450°C-based Pyrolysis-GC/MS showed that 42 peaks were obtained from the 450°C pyrolyzate of benzene/ethanol-extracted residues of oil-tea cake, and 41 compounds representing 97.53% of the total areas were identified. The analytical result revealed that the main components of benzene/ethanol-extracted residues of oil-tea cake by 450°C-based pyrolysis- GC/MS were as: Ethanone, 1-(2-Hydroxy-5-Methylphenyl)- (19.16%), Phenol, 2-Methoxy-6-(2-Propenyl)- (15.24%), Mequinol (14.37%), 2-Cyclohexen-1-One, 4,4,6-Trimethyl- (6.51%), 1,2-Cyclobutanedicarboxylic Acid, Trans- (5.68%), 3-Tert-Butyl-4-Hydroxyanisole (4.92%), Phenol, 2-Methoxy-4-Methyl- (4.33%), Phenol, 4-Ethyl-2-Methoxy- (3.62%), Vanillin (3.59%), Phenol, 2,6-Dimethoxy-4- (2-Propenyl)- (3.17%), N,N-Dimethyl-2-Cyclohexyloxyethylamine (2.94%), 1,3-Cyclopentanedione, 2-Methyl- (2.85%), Eugenol (2.56%), etc. The results of function analyses showed that the benzene/ethanol-extracted residues of oil-tea cake contain abundant components of rare natural medicinal materials, and materials of high-grade spice, cosmetic and food industry.
In order to better utilize and recover the productive waste leaves from the Cinnamomum camphora, pyrolysis- GC/MS technology was used to analyze the possible top value-added components of benzene/ethanol extractives of Cinnamomum camphora leaves. Relative content of each component was determined by area normalization. 95 compounds from 102 peaks representing 99.216% of the benzene/ethanol extractives of Cinnamomum camphora leaves were identified, and the main constituents were Hexadecanoic acid, 4-nitrophenyl ester (17.336%), Vitamin E (4.804%), Oxirane, hexadecyl- (4.639%), 2,6-Bis(3,4-methylenedioxyphenyl) -3,7-dioxabicyclo(3.3.0)octane (4.333%), 1-Hexacosene (4.148%), Hexadecanoic acid, 2-methoxy-, methyl ester (3.783%), 1,19-Eicosadiene (3.607%), 3-Cyclohexene-1- methanol, .alpha.,.alpha.4-trimethyl- (3.542%), .gamma.-Sitosterol (3.495%), Nonacosane (3.217%), .gamma.-Tocopherol (3.119%), Eucalyptol (2.23%), vanillin (2.742%), Heptacosane (2.182%), Pentatriacontane (2.039%), 1-Nonadecene (2.011%), etc. The results of function analyses showed that the 350 °C pyrolyzate from benzene/ethanol extractives of waste leaves of Cinnamomum camphora are abundant in materials of noble natural medicines and cosmetic.
Py-GC/MS technology was used to analyze the high-grade resource recovering approaches of C. camphora root wood at 350°C. The result showed that the chemical components of acetone extractives from C. camphora root wood are as: Benzene, 1,2-dimethoxy-4-(2-propenyl)- (10.255%), Bicyclo[2.2.1]heptan-2-one, 1,7,7-trimethyl-, (1R)- (7.751%), p-menth-1-en-8-ol (5.765%), Phenol, 2,6-dimethoxy-4-(2-propenyl)- (3.833%), 1,6-Cyclodecadiene, 1-methyl-5-methylene-8- (1-methylethyl)-, [s-(E,E)]- (3.669%), D-Allose (3.265%), Acetic acid (2.784%), 1(2H)-Naphthalenone, octahydro-8a-hydroxy- (2.719%), 1,3-Benzodioxole, 4-methoxy-6- (2-propenyl)- (2.674%), .beta.(3,4-Methylenedioxyphenyl)propionic acid (2.216%), Phenol, 4-methyl- (2.200%), Phenol, 2,6-dimethoxy- (2.138%), 3,4-Methylenedioxyphenyl acetone (2.125%), 5-Hepten-2-one, 6-methyl- (2.075%), 2-Oxabicyclo[2.2.2]octan-6-ol, 1,3,3-trimethyl- (1.808%), Phenol, 2-methoxy-3-(2-propenyl)- (1.688%), etc. The analytical result by 350°C-based Py-GC/MS showed that the 350°C pyrolyzate of acetone extractives from C. camphora root wood can be used as top value-added materials of biomedicine, but also used as the bioactive materials of bioenergy, cosmetic, food, and other industrial solvents.
In order to evaluate its potential biomedicines, the extractives of Phyllostachys pubescens were extracted and determined by Py-GC-MS. And the main constituents were 1-phenanthrenecarboxylic acid, 1,2,3,4,4a,9,10,10a-octahydro-1,4a-dimethyl-7-(1-methylethyl)-(% 7.02), stigmast-5-en-3-ol, oleate(4.33%), 4,4,6a,6b,8a,11,11,14b-octamethyl-1,4,4a,5,6,6a,6b,7,8, 8a,9,10,11,12,12a,14,14a,14b-octadecahydro-2h-picen-3-one(3.39%), etc. So the benzene-alcohol extractives of Phyllostachys pubescens could be used for biomedical engineering.
Liriodendron chinense (Hemsl.) Sarg (Chinese tulip tree) has a long history of utilization and plantation, but the chemical components of benzene/ethanol extractives of Liriodendron chinense (Hemsl.) Sarg leaves were unrevealed. The analytical result by method of GC/MS showed that the chemical components of benzene/ethanol extractives of freeze-dried Liriodendron chinense were identified as 55 constituent, and the main components are as: 2-Propenenitrile, 2-chloro- (13.75%), 1-Mercapto-2-heptadecanon (13.10 %), 1-Mercapto-2-heptadecanon (12.77%), Ethanol, 2-butoxy- (12.03%), 1-Docosanol (10.74%), Guanidine, (4-aminobutyl)- (5.05%), 5,10-Pentadecadiyn-1-ol, acetate (4.82%), 1,2,4-Butanetriol (3.13%), Thiophene, 2-ethyltetrahydro- (2.09%), 1-Eicosanol (2.00%), 1-Butanol, 3-methyl-, formate (1.60%), Butanoic acid (1.60%), .alpha.-D-Xylofuranoside, methyl 3,5-di-O-methyl- (1.30%), Phenol, 2,6-dimethoxy-4-(2-propenyl)- (1.29%),5.alpha.-Pregnane-12,20-dione (1.12%), Cyclopentanol (0.82%), etc. As the first report here, our result by GC/MS showed that the benzene-methanol extractive of freeze-dried leaves from Liriodendron chinense (Hemsl.) Sarg can be developed into top value-added materials of medicines and spicery.
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