Friction stir processing (FSP) is a novel severe plastic deformation technique developed in recent years to produce fine-grained structural materials. Through increasing the processing pass, further grain refinement can be achieved. In this paper, the microstructure and mechanical properties of AZ91 magnesium alloy prepared by the single-pass and two-pass FSP were studied. The results showed that the coarse, network-like eutectic β-Mg17Al12 phase was broken into particles and some of them dissolved into the magnesium matrix, and the α-Mg grains were remarkably refined after FSP. The average grain sizes of the single-pass and two-pass FSP alloys were 8.3 μm and 5.8 μm respectively. The ultimate tensile strengths of the specimens were 284.5 MPa and 319.7 MPa, and elongations were 13% and 14.5%, respectively. The improved mechanical properties of the two-pass FSP specimen were mainly attributed to the finer grain size and more homogenized microstructure.
Friction stir processing (FSP) is a novel severe plastic deformation technique developed in recent years to produce fine-grained structural materials. In this paper, the microstructure and mechanical properties of ZK60 magnesium alloy prepared by the single-pass and two-pass FSP were studied. The first-pass was subjected with 800r/min-100mm/min and the second-pass was subjected with 600r/min-100mm/min. The results show that the coarse second phase was dissolved into magnesium matrix and the α-Mg grains were remarkably refined in stir zone after FSP. The average grain sizes of the single-pass and two-pass FSP alloys were 6.8μm and 6.0μm respectively. The microhardnesses of the specimens were 70HV and 65HV, the ultimate tensile strengths were 276MPa and 272MPa, and the elongations were 31.6% and 42.5%, respectively. Through increasing the processing pass, the microstructure became finer and the second phase is dissolved more thoroughly. The combined effect of grain refinement and second phase dissolved was responsible for the change of mechanical properties.
AZ31 magnesium alloy was friction stir spot welded in air and cooling in water. The effect of the enhanced cooling rate on the microstructure and mechanical properties of the joint was analyzed. The results showed that flowing water had obvious cooling effect instantaneously, which significantly restrained the growth of dynamic recrystallized grains. The average grain size in stir zone was 1.3μm in cooling water condition, which is far smaller than that of the joint prepared in air cooling condition. Under the condition of enhanced cooling, the microhardness in stir zone significantly increased, the ultimate tensile load (~ 3.99kN) increased by 15.7%, and the tensile deformation value (~ 3.65 mm) increased by 62.2%. Dimples in SEM fracture morphologies indicated the better plastic deformation capacity of joints prepared by cooling water, which failed through a mixture mode of ductile and brittle fracture.
Mg-2.5wt%Y-4wt%Nd-0.5wt%Zr casting alloy was subjected to submerged friction stir processing (SFSP) with different rotation rates (ω) and travel speeds (υ). The influence of the ratio of ω/υ on the microstructure and mechanical properties of Mg-Y-Nd alloy was investigated in the present work by optical microscopy, scanning electron microscopy, transmission electron microscopy, tensile test and hardness measurement. The results showed that the average grain sizes of SFSP samples were significantly refined compared with as-cast sample, and the coarse net-shaped Mg12Nd phases which located at grain boundaries in as-cast sample were changed into small particles. The combined effect of grain refinement and uniform particles distribution was responsible for the enhancement of mechanical properties. The relative optimal parameter of 600 rpm/60 mm·min-1in this research obtained the finest grain size and the best mechanical properties, which were 1.1 μm for average grain size, 305 MPa for ultimate tensile strength and 22% for elongation, respectively.
The effects of heat treatment on the microstructures and mechanical properties of a squeeze-casted Al-6.8%Zn-2.7%Mg-2.0%Cu alloy were studied by optical microscopy (OM), scanning electron microscopy (SEM) and X-ray diffraction (XRD). It is found that squeeze casting can refine the microstructure of the alloy markedly accelerates the diffusion process of solute atoms during solution heat treatment. After solution heat treatment at 470°C for 10h and artificial aging at 130°C for 24h, the tensile strength and the elongation of the squeeze-casted alloy reach 590MPa and 5.0%, respectively, which are almost equal to those of the wrought alloy, and are significantly higher than those of the gravity-casted alloy (435MPa and 1.3%). Based on the experimental results, the mechanism of microstructural evolution and the effect of squeeze casting on the kinetics of solute diffusion and aging precipitation of the squeeze-casted Al-Zn-Mg-Cu alloy were discussed.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.
customersupport@researchsolutions.com
10624 S. Eastern Ave., Ste. A-614
Henderson, NV 89052, USA
Copyright © 2024 scite LLC. All rights reserved.
Made with 💙 for researchers
Part of the Research Solutions Family.