The crystal structure of Gel 4 was refined using 100 Κ and 297 Κ X-ray data. Gel 4 crystallizes in the cubic space group P2i/a3 (No 205) with a = 11.861(1) A at 100 Κ and 12.0303(6) Ä at 297 K. Analysis of the displacement parameters gives no hint for rigid body motion.
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