As-grown Co 49 Ni 21 Ga 30 [001]-and [123]-oriented single crystals were subjected to cyclic compression loading at room temperature above the austenite finish temperature of 15°C. Straincontrolled experiments were performed using both incremental strain steps and constant strain amplitudes. Cyclic deformation with a maximum strain amplitude of 2.5 pct resulted in rapid accumulation of irrecoverable strains in the [123]-oriented crystals. However, after a few cycles, the samples demonstrated cyclic stability with fully recoverable transformation. By contrast, the [001]-oriented crystals displayed excellent cyclic stability with hardly any change in stress-strain characteristics. In-situ optical microscopy and electron backscattered diffraction analysis were employed to clarify the events that take place at different stages of a typical loading-unloading history. The in-situ observations also revealed that the initiation and growth characteristics of stress-induced martensite (SIM) are heterogeneous on the microscopic scale in CoNiGa alloys. In addition, theoretical transformation and detwinning strains, and resolved shear stress factors (RSSFs), were calculated based on the energy minimization theory and are compared to the experimentally obtained orientation-dependent transformation stress and strain levels. It is shown that the selection of an appropriate orientation is one of the key criteria to optimize the pseudoelastic (PE) response and cyclic stability of CoNiGa alloys.
The tensile deformation response and texture evolution of aluminum alloyed Hadfield steel single crystals oriented in the h1 6 9i direction is investigated. In this material, the strain hardening response is governed by the high-density dislocation walls (HDDWs) that interact with glide dislocations. A microstructure-based visco-plastic self-consistent model was modified to account for mechanical twinning in addition to the prevailing contribution of the HDDWs. Simulations revealed the contribution of twinning to the overall work hardening at the later stages of deformation. Moreover, both the deformation response and the rotation of the loading axis associated with plastic flow are successfully predicted even at the high-strain levels attained (0.53). Predicting the texture evolution serves as a separate check for validating the model, motivating its utilization in single and polycrystals of other alloys that exhibit combined HDDWs and twinning. Motivation and significanceIn a recent study investigating the strain hardening response of aluminum alloyed Hadfield steel (HSwAl), we attributed the unusually high-strain hardening coefficients (%G/23 1 ) observed in the single crystals of this alloy to the formation of high-density dislocation walls (HDDWs) (Canadinc et al., 2005). Aluminum was added to Hadfield steel at 2.58 wt%, which normally has a chemical composition of 13.93 wt% Mn, 1.30 wt% C and balance Fe. The resulting material (HSwAl) with a face-centered cubic (fcc) structure at room temperature displayed HDDWs that form and evolve as a result of plastic deformation. The interaction 0020-7683/$ -see front matter Ó
The general trend in oil and gas industry gives a clear direction towards the need for high strength grades up to X100. The exploration in extreme regions and under severe conditions, e.g. in ultra deep water regions also considering High Temperature/High Pressure Fields or arctic areas, becomes more and more important with respect to the still growing demand of the world for natural resources. Further, the application of high strength materials enables the possibility of structure weight reduction which benefits to materials and cost reduction and increase of efficiency in the pipe line installation process. To address these topics, the development of such high strength steel grades with optimum combination of high tensile properties, excellent toughness properties and sour service resistivity for seamless quenched and tempered pipes are in the focus of the materials development and improvement of Vallourec. This paper will present the efforts put into the materials development for line pipe applications up to grade X100 for seamless pipes manufactured by Pilger Mill. The steel concept developed by Vallourec over the last years [1,2] was modified and adapted according to the technical requirements of the Pilger rolling process. Pipes with OD≥20″ and wall thickness up to 30 mm were rolled and subsequent quenched and tempered. The supportive application of thermodynamic and kinetic simulation techniques as additional tool for the material development was used. Results of mechanical characterization by tensile and toughness testing, as well as microstructure examination by light-optical microscopy will be shown. Advanced investigation techniques as scanning electron microcopy and electron backscatter diffraction are applied to characterize the pipe material up to the crystallographic level. The presented results will demonstrate not only the effect of a well-balanced alloying concept appointing micro-alloying, but also the high sophisticated and precise thermal treatment of these pipe products. The presented alloying concept enables the production grade X90 to X100 with wall thickness up to 30 mm and is further extending the product portfolio of Vallourec for riser systems for deepwater and ultra-deep water application [1, 3, 4].
The challenging exploration conditions appearing in ultra deep offshore projects promoted the development of high strength linepipe steel grades with yield strength of 80 ksi and higher in recent years. With increasing strength more attention has to be paid to welding procedures to realise the required mechanical properties of the weld seam. The combination of demanding toughness requirements at low temperatures and adequate corrosion resistance of welded joints is a key for complex deep offshore riser and linepipe applications. The welding process was optimised by Vallourec with respect to heat input and preheating temperature for joining seamless quenched and tempered pipes in grade X80. A root welding strategy has been developed particularly with regards to sour service applications. Extensive mechanical test results including Charpy impact testing, hardness, CTOD and SSC testing will be presented. In addition Gleeble trials were carried out using different thermal cycles to simulate multilayer welding. The aim was to improve the understanding of the base material behaviour in the heat affected zone (HAZ) during welding. The microstructure was characterized by LOM, SEM and furthermore hardness and Charpy impact tests were executed. Based on the gathered knowledge and test results welding recommendations and welding strategies for high strength steel X80 seamless line pipes are deduced.
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