Crack progression during compressive sustained-peak low-cycle fatigue (SPLCF) was examined in vapor phase aluminide coated single-crystal Ni-base superalloy Rene´N5. Strain-controlled tests with a 120-second hold at compression were conducted at 1366 K (1093°C) with A = -1 (R = -¥) and 0.35 pct total strain range, and were terminated at selected fractions of predicted life. Crack lengths on the surface and crack depth in longitudinal sections were examined for each specimen. All cracks appeared to have initiated at the coating surface. Failed specimens showed that cracks initially grew on (001), perpendicular to the stress axis, and then deflected to other crystallographic planes. Interrupted test specimens showed crevices initiated on the coating surface at less than 10 pct of the predicted life. The depths of crevices into the coating increased with cyclic exposure, but they did not penetrate into the substrate through the interdiffusion zone (IDZ) until about 80 pct of predicted life. Stress relaxation during compressive hold results in residual tension upon unloading. These results suggest that improving creep resistance of the substrate alloy and developing a coating system that can delay crack penetration into the substrate are keys for improved SPLCF life.
Titanium aluminide alloys with compositions near Ti-25A1-25Nb at.% were prepared by both rapid solidification and ingot techniques. Their tensile and creep properties were studied after heat treatment to produce various microstructures containing ordered orthorhombic (O) [1], ordered beta (βo), and α2 phases. It was found that these alloys had higher specific strength from room temperature to 760°C than conventional α2 alloys. Ductility and tensile strength of O+βo alloys were strongly dependent upon heat treatment, with the highest strength observed as-heat-treated, and the highest ductility after long term aging. The creep resistance of single phase O and two phase O+βo alloys was strongly dependent upon heat treatment.
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