We present experimental results obtained with a cryogenically cooled, high-resolution x-ray spectrometer based on a 141 μm×141 μm Nb-Al-Al2O3-Al-Nb superconducting tunnel junction (STJ) detector in a demonstration experiment. Using monochromatized synchrotron radiation we studied the energy resolution of this energy-dispersive spectrometer for soft x rays with energies between 70 and 700 eV and investigated its performance at count rates up to nearly 60 000 cps. At count rates of several 100 cps we achieved an energy resolution of 5.9 eV (FWHM) and an electronic noise of 4.5 eV for 277 eV x rays (the energy corresponding to C K). Increasing the count rate, the resolution 277 eV remained below 10 eV for count rates up to ∼10 000 cps and then degraded to 13 eV at 23 000 cps and 20 eV at 50 000 cps. These results were achieved using a commercially available spectroscopy amplifier with a baseline restorer. No pile-up rejection was applied in these measurements. Our results show that STJ detectors can operate at count rates approaching those of semiconductor detectors while still providing a significantly better energy resolution for soft x rays. Thus STJ detectors may prove very useful in microanalysis, synchrotron x-ray fluorescence (XRF) applications, and XRF analysis of light elements (K lines) and transition elements (L lines).
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Superconducting tunnel junctions coupled to superconducting absorbers may be used as high-resolution, high-efficiency X-ray s p e ctrometers. We have tested devices with niobium Xray absorbing layers coupled to aluminum layers that serve as quasiparticle traps. In this work we measure the current pulses from a large-area tunnel junction using an amplifier based on an array of 100 SQUIDS. Using this amplifier and a 282 ym x 2 8 2 ym junction, we have measured an energy resolution of 19 eV FWHM for 1.5 keV X rays and 21 eV for 2.6 keV X rays. The area of this junction is eight t i m e s the area of any junction previously measured t o have such high energy resolution.
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