High-temperature piezoelectric crystals, including YCa4O(BO3)3, LiNbO3, and AlN, have been studied for use in ultrasonic transducers under continuous operation for 55 h at 550°C. Additionally, thermal ratcheting tests were performed on the transducers by subjecting the crystals to heat treatments followed by ultrasonic performance testing at room temperature and 500°C. The changes resulting from the heat treatments were less than the statistical spread obtained in repeated experiments and were thus considered negligible. Finally, in situ measurements of the pulse-echo response of YCa4O(BO3)3 were performed at temperatures up to 950°C for the first time, showing stable characteristics up to these high temperatures.
For practical use in harsh radiation environments, we pose selection criteria for piezoelectric materials for non-destructive evaluation (NDE) and material characterization. Using these criteria, piezoelectric aluminum nitride is shown to be an excellent candidate. The results of tests on an aluminum-nitride- based transducer operating in a nuclear reactor are also presented. We demonstrate the tolerance of single-crystal piezoelectric aluminum nitride after fast and thermal neutron fluences of 1.85 x 10(18) neutron/cm(2) and 5.8 x 10(18) neutron/ cm(2), respectively, and a gamma dose of 26.8 MGy. The radiation hardness of AlN is most evident from the unaltered piezoelectric coefficient d33, which measured 5.5 pC/N after a fast and thermal neutron exposure in a nuclear reactor core for over 120 MWh, in agreement with the published literature value. The results offer potential for improving reactor safety and furthering the understanding of radiation effects on materials by enabling structural health monitoring and NDE in spite of the high levels of radiation and high temperatures, which are known to destroy typical commercial ultrasonic transducers.
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