This study focused on investigating the adhesion and tribological properties of niobium-doped titanium nitride (TiNbN) coatings deposited on D2 steel substrates at various substrate temperatures (Ts) under simulated cutting conditions. X-ray diffraction confirmed the presence of coatings with an FCC crystalline structure, where Nb substitutes Ti atoms in the TiN lattice. With increasing Ts, the lattice parameter decreased, and the crystallite material transitioned from flat-like to spherical shapes. Nanoindentation tests revealed an increase in hardness (H) with Ts, while a decrease in the elastic modulus (E) resulted in an improved elastic strain limit for failure (H/E) and plastic deformation resistance (H3/E2), thereby enhancing stiffness and contact elasticity. Adhesion analysis showed critical loads of ~50 N at Ts of 200 and 400 °C, and ~38 N at Ts of 600 °C. Cohesive failures were associated with lateral cracking, while adhesive failures were attributed to chipping spallation. The tribological behavior was evaluated using a pin-on-disk test, which indicated an increase in friction coefficients with Ts, although they remained lower than those of the substrate. Friction and wear were influenced by the surface morphology, facilitating the formation of abrasive particles. However, the absence of coating detachment in the wear tracks suggested that the films were capable of withstanding the load and wear.
Precision agriculture has greatly benefited from advances in machine vision and image processing techniques. The use of feature descriptors and detectors allows to find distinctive keypoints in an image and the use of this approach for agronomical applications has become a widespread field of study. By combining near infrared (NIR) images, acquired with a modified Nikon D80 camera, and visible spectrum (VIS) images, acquired with a Nikon D300s, a proper crop identification could be obtained. Still, the use of different sensors brings an image matching challenge due to the difference between cameras and the possible distortions from each imaging technique. The aim of this paper is to compare the performance of several feature descriptors and detectors by comparing near infrared and visual spectral bands in rice crop images. Therefore, a group of 20 different scenes with different cameras and growth stages in a rice crop were evaluated. Thus, red, green, blue (RGB) and L, a, b (CIE L*a*b*) channels were extracted from VIS images in order to compare the matches obtained between each of them and the corresponding NIR image. The BRISK, SURF, SIFT, ORB, KAZE, and AKAZE methods were implemented, which act as descriptors and detectors. Additionally, a combination was made between the FAST algorithm for the detection of keypoints with the BRIEF, BRISK, and FREAK methods for features description. BF and FLANN matching methods were used. The algorithms were implemented in Python using OpenCV library. The green channel presented the highest number of correct matches in all methods. In turn, the method that presented the highest performance both in time and in the number of correct matches was the combination of the FAST feature detector and the BRISK descriptor.
The study of material hardness is crucial for determining its quality, potential failures, and appropriate applications, as well as minimizing losses incurred during the production process. To achieve this, certain criteria must be met to ensure high quality. This process is typically performed manually or using techniques based on analyzing indentation image patterns produced through the Vickers hardness technique. However, these techniques require that the indentation pattern is not aligned with the image edges. Therefore, this paper presents a technique based on convolutional neural networks (CNNs), specifically, a YOLO v3 network connected to a Dense Darknet-53 network. This technique enables the detection of indentation corner positions, measurement of diagonals, and calculation of the Vickers hardness value of D2 steel treated thermally and coated with Titanium Niobium Nitride (TiNbN), regardless of their position within the image. By implementing this architecture, an accuracy of 92% was achieved in accurately detecting the corner positions, with an average execution time of 6 seconds. The developed technique utilizes the network to detect the regions containing the corners and subsequently accurately determines the pixel coordinates of these corners, achieving an approximate relative percentage error between 0.17% to 5.98% in the hardness results.
Hardness is one of the most important mechanical properties of materials, since it is used to estimate their quality and to determine their suitability for a particular application. One method of determining quality is the Vickers hardness test, in which the resistance to plastic deformation at the surface of the material is measured after applying force with an indenter. The hardness is measured from the sample image, which is a tedious, time-consuming, and prone to human error procedure. Therefore, in this work, a new automatic method based on image processing techniques is proposed, allowing for obtaining results quickly and more accurately even with high irregularities in the indentation mark. For the development and validation of the method, a set of microscopy images of samples indented with applied forces of 5N and 10N on AISI D2 steel with and without quenching, tempering heat treatment and samples coated with titanium niobium nitride (TiNbN) was used. The proposed method was implemented as a plugin of the ImageJ program, allowing for obtaining reproducible Vickers hardness results in an average time of 2.05 seconds with an accuracy of 98.3% and a maximum error of 4.5% with respect to the values obtained manually, used as a golden standard.
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